Molecularly imprinted polymer cartridges coupled to liquid chromatography for simple and selective analysis of penicilloic acid and penilloic acid in milk by matrix solid-phase dispersion

Luo, Zhimin; Du, Wei; Zheng, Penglei; Guo, Pengqi; Wu, Ningli; Tang, Weibing; Zeng, Aiguo; Chang, Chun; Fu, Qiang

doi:10.1016/j.fct.2015.05.014

Cited by 22 publications

(9 citation statements)

References 53 publications

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“…For instance, MIPs were set up on carbon nanotubes (CNTs) for the MSPD readiness of malachite green in amphibian items [117]. Silica gel [118], silica nanoparticles [119], and mesoporous silica [120] equally have been accounted for as the bearer of MIPs to improve the selectivity of MSPD sorbents. In addition, Wang et al explained the combination of blended layout MIPs for the extraction of multi-class veterinary medications [121].…”

Section: Recent Advances In Mspd Sorbentmentioning

confidence: 99%

Mi-Spe, M-Spe and M-SPD Recent Application on Solid Phase Extraction for Compound Extraction of Complex Matrices

Gopalan

Hasanah

2019

Int J App Pharm

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Solid Phase Extraction is a method used for extraction, purification of compounds contained in complex matrices and purification of samples in the fields of industry, pharmacy, and toxicology analysis. This review represents the recent advances of solid phase extraction from different mode of separation which are the most commonly used in recent days such as molecular imprinting solid phase extraction (MISPE), magnetic solid phase extraction (MSPE) and matrix solid phase dispersion (MSPD). In this review, the applications of MISPE in the analysis of agrochemicals such as herbicides, fungicides and insecticides are summarized. This review also states preparation of various magnetic composites (MSPE) based on graphene and its application as adsorbents in pre concentrating natural mixes, organic macromolecules. Besides this, this review summarizes the application of MSPD in biological, food, and environmental samples, including both organic and inorganic analyte.

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Section: Recent Advances In Mspd Sorbentmentioning

confidence: 99%

Mi-Spe, M-Spe and M-SPD Recent Application on Solid Phase Extraction for Compound Extraction of Complex Matrices

Gopalan

Hasanah

2019

Int J App Pharm

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“…Furthermore, the authors compared the developed MSPD protocol with three commercially available SPE cartridges, Cleanert PAX (500 mg, 6 mL), Cleanert PCX (500 mg, 6 mL) and Cleanert Florisil (500 mg, 6 mL) purchased from Bonna-Agela Technologies Inc. (Newark, USA), in terms of selectivity and extraction efficiency. The MSPD protocol displayed highest recoveries than the SPE protocols, with 88.5% recovery for penicilloic acid and 85.9% for penilloic acid [ 64 ]. All the reported applications are summarized in Table 2 .…”

Section: Mip Applications For the Extraction Of Antibiotics In Milmentioning

confidence: 99%

Molecularly Imprinted Polymers as Extracting Media for the Chromatographic Determination of Antibiotics in Milk

Bitas

Samanidou

2018

Molecules

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Milk-producing animals are typically kept stationary in overcrowded large-scale farms and in most cases under unsanitary conditions, which promotes the development of infections. In order to maintain sufficient health status among the herd or promote growth and increase production, farmers administer preventative antibiotic doses to the animals through their feed. However, many antibiotics used in cattle farms are intended for the treatment of bacterial infections in humans. This results in the development of antibiotic-resistant bacteria which pose a great risk for public health. Additionally, antibiotic residues are found in milk and dairy products, with potential toxic effects for the consumers. Hence the need of antibiotic residues monitoring in milk arises. Analytical methods were developed for the determination of antibiotics in milk, with key priority given to the analyte extraction and preconcentration step. Extraction can benefit from the production of molecularly imprinted polymers (MIPs) that can be applied as sorbents for the extraction of specific antibiotics. This review focuses on the principals of molecular imprinting technology and synthesis methods of MIPs, as well as the application of MIPs and MIPs composites for the chromatographic determination of various antibiotic categories in milk found in the recent literature.

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“…The kinetic adsorption test was carried out by using EMIPs or ENIPs (20 mg) that were dispersed in the E1 aqueous solution (10 mL) and shaken at room temperature for different time (5,10,15,20,30,45,60,90, and 120 min), and then filtered. The supernatant was measured by HPLC and the adsorption capacity was calculated.…”

Section: Adsorption Testmentioning

confidence: 99%

Facile preparation of polydopamine‐coated imprinted polymers on the surface of SiO₂ for estrone capture in milk samples

Zheng

Zhang

Luo

et al. 2016

J of Separation Science

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Estrone molecularly imprinted polymers were synthesized through the self-polymerization of dopamine on the surface of silica gels, which had the characteristics of mild polymerization conditions, simple reaction procedure and good specific recognition ability for estrone. The estrone molecularly imprinted polymers were characterized by scanning electron microscopy, Fourier transform infrared spectroscopy, thermogravimetric analysis, elemental analysis and nitrogen adsorption-desorption tests. The characterization confirmed that the imprinted polymers were successfully grafted on the surface of silica gels. Through investigating the adsorption performance, the prepared estrone molecularly imprinted polymers exhibited high adsorption capacity, fast mass transfer, as well as excellent selectivity toward estrone. The estrone molecularly imprinted polymers as the solid-phase extraction adsorbent coupled with high-performance liquid chromatography was developed to determine estrone from the milk samples. The developed estrone molecularly imprinted polymer solid-phase extraction with high-performance liquid chromatography method exhibited satisfactory specificity, precision, accuracy and good linearity relationship in the range of 0.2-20 μg/mL. The developed method is simple, fast, effective and high specificity method and it provides a new method to detect the residues of estrone in animal foods.

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Molecularly imprinted polymer cartridges coupled to liquid chromatography for simple and selective analysis of penicilloic acid and penilloic acid in milk by matrix solid-phase dispersion

Cited by 22 publications

References 53 publications

Mi-Spe, M-Spe and M-SPD Recent Application on Solid Phase Extraction for Compound Extraction of Complex Matrices

Mi-Spe, M-Spe and M-SPD Recent Application on Solid Phase Extraction for Compound Extraction of Complex Matrices

Molecularly Imprinted Polymers as Extracting Media for the Chromatographic Determination of Antibiotics in Milk

Facile preparation of polydopamine‐coated imprinted polymers on the surface of SiO₂ for estrone capture in milk samples

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Molecularly imprinted polymer cartridges coupled to liquid chromatography for simple and selective analysis of penicilloic acid and penilloic acid in milk by matrix solid-phase dispersion

Cited by 22 publications

References 53 publications

Mi-Spe, M-Spe and M-SPD Recent Application on Solid Phase Extraction for Compound Extraction of Complex Matrices

Mi-Spe, M-Spe and M-SPD Recent Application on Solid Phase Extraction for Compound Extraction of Complex Matrices

Molecularly Imprinted Polymers as Extracting Media for the Chromatographic Determination of Antibiotics in Milk

Facile preparation of polydopamine‐coated imprinted polymers on the surface of SiO2 for estrone capture in milk samples

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Facile preparation of polydopamine‐coated imprinted polymers on the surface of SiO₂ for estrone capture in milk samples