Multi-response optimization of factors affecting ultrasonic assisted extraction from Iranian basil using central composite design

Izadiyan, Parisa; Hemmateenejad, Bahram

doi:10.1016/j.foodchem.2015.06.036

Cited by 86 publications

(47 citation statements)

References 32 publications

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“…It is a relatively simple method suitable for determination of antiradical activity of a large number of natural extracts in relatively short time, which makes this model one of the most commonly used in literature. [12,13,24] …”

Section: Radical Scavenging Activity Of the Extractsmentioning

confidence: 99%

“…Therefore, the extraction conditions must be carefully selected to ensure the extract of desired characteristics of the prepared extracts. [12] An efficient extraction process should maximize the recovery of target compounds with minimal degradation, resulting in an extract with high biological activity. Ideally, this should be accomplished using environmentally friendly technologies and low-cost raw materials and solvents.…”

Section: Introductionmentioning

confidence: 99%

“…Ideally, this should be accomplished using environmentally friendly technologies and low-cost raw materials and solvents. [12] To achieve this, a fine-tuning of the experimental conditions is often needed, which requires a large number of experiments to be performed. Response surface methodology (RSM) is a collection of mathematical and statistical techniques for modeling and optimization of complex processes.…”

Section: Introductionmentioning

confidence: 99%

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Multi-response Optimization of Ultrasound-assisted Extraction of Bioactive Components from Medicago Sativa L.

2017

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Response surface methodology was used to optimize experimental conditions for ultrasound-assisted extraction of functional components from Medicago sativa L. (Fabaceae) aerial parts. The procedure was performed according to the Box-Behnken design. The independent variables were ethanol concentration (X1), temperature (X2), and pH (X3), while the responses were extraction yield, DPPH radical scavenging activity of the extracts (RSA IC50), content of total phenols (TP), total flavonoids (TF) and total phenolic acids (TPA). The response values of the extracts prepared at optimum conditions (X1, X2, X3) were: yield (162 mg/ml, 20 %, 60 °C, 5.5), TP (6.63 mg/ml, 100 %, 60 °C, 5.5), TF (0.292 mg/ml, 100 %, 23 °C, 5.5), TPA (0.275 mg/ml, 100 %, 23 °C, 8.5) and RSA IC50 (3.97 mg/ml, 40 %, 60 °C, 7.0). The predicted values matched well with the observed ones indicating the suitability of the selected models for extraction of bioactive compounds from M. sativa.

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Section: Radical Scavenging Activity Of the Extractsmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

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Multi-response Optimization of Ultrasound-assisted Extraction of Bioactive Components from Medicago Sativa L.

2017

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“…It has the sufficient power to break up the plant cells and the high contact surface between both liquids, which speeds up mass transfer from sample solution to extractive solvent [10,11]. Nowadays, the UAE method has been successfully applied to extract of bioactive compounds from natural products and environmental analysis [12][13][14][15][16][17][18].…”

Section: Introductionmentioning

confidence: 99%

Rapid determination of the volatile components in tobacco by ultrasound‐microwave synergistic extraction coupled to headspace solid‐phase microextraction with gas chromatography‐mass spectrometry

Yang

Chu

Guang-hong

et al. 2016

J of Separation Science

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An ultrasound-microwave synergistic extraction coupled to headspace solid-phase microextraction was first employed to determine the volatile components in tobacco samples. The method combined the advantages of ultrasound, microwave, and headspace solid-phase microextraction. The extraction, separation, and enrichment were performed in a single step, which could greatly simplify the operation and reduce the whole pretreatment time. In the developed method, several experimental parameters, such as fiber type, ultrasound power, and irradiation time, were optimized to improve sampling efficiency. Under the optimal conditions, there were 37, 36, 34, and 36 components identified in tobacco from Guizhou, Hunan, Yunnan, and Zimbabwe, respectively, including esters, heterocycles, alkanes, ketones, terpenoids, acids, phenols, and alcohols. The compound types were roughly the same while the contents were varied from different origins due to the disparity of their growing conditions, such as soil, water, and climate. In addition, the ultrasound-microwave synergistic extraction coupled to headspace solid-phase microextraction method was compared with the microwave-assisted extraction coupled to headspace solid-phase microextraction and headspace solid-phase microextraction methods. More types of volatile components were obtained by using the ultrasound-microwave synergistic extraction coupled to headspace solid-phase microextraction method, moreover, the contents were high. The results indicated that the ultrasound-microwave synergistic extraction coupled to headspace solid-phase microextraction technique was a simple, time-saving and highly efficient approach, which was especially suitable for analysis of the volatile components in tobacco.

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“…The Box-Behnken design (BBD), one of the most used RSM methods, plays a pivotal role in arranging and interpreting the optimal experiments. Currently, multiple literatures have reported that ultrasound-assisted extraction with RSM is commonly applied in analyzing bioactive components of plants, such as Chrysanthemum morifolium flower heads [6], Ligusticum rhizomes [7], sweet basil [8], and sugar beet [9].…”

Section: Introductionmentioning

confidence: 99%

Ultrasound-Assisted Extraction, Antioxidant and Anticancer Activities of the Polysaccharides from Rhynchosia minima Root

Jia

Zhang

et al. 2015

Molecules

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Box-Behnken design (BBD), one of the most common response surface methodology (RSM) methods, was used to optimize the experimental conditions for ultrasound-assisted extraction of polysaccharides from Rhynchosia minima root (PRM). The antioxidant abilities and anticancer activity of purified polysaccharide fractions were also measured. The results showed that optimal extraction parameters were as follows: ultrasound exposure time, 21 min; ratio of water to material, 46 mL/g; ultrasound extraction temperature, 63˝C. Under these conditions, the maximum yield of PRM was 16.95%˘0.07%. Furthermore, the main monosaccharides of purified fractions were Ara and Gal. PRM3 and PRM5 exhibited remarkable DPPH radical scavenging activities and reducing power in vitro. PRM3 showed strong inhibitory activities on the growth of MCF-7 cells in vitro. The above results indicate that polysaccharides from R. minima root have the potential to be developed as natural antioxidants and anticancer ingredients for the food and pharmaceutical industries.

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Multi-response optimization of factors affecting ultrasonic assisted extraction from Iranian basil using central composite design

Cited by 86 publications

References 32 publications

Multi-response Optimization of Ultrasound-assisted Extraction of Bioactive Components from Medicago Sativa L.

Multi-response Optimization of Ultrasound-assisted Extraction of Bioactive Components from Medicago Sativa L.

Rapid determination of the volatile components in tobacco by ultrasound‐microwave synergistic extraction coupled to headspace solid‐phase microextraction with gas chromatography‐mass spectrometry

Ultrasound-Assisted Extraction, Antioxidant and Anticancer Activities of the Polysaccharides from Rhynchosia minima Root

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