2020
DOI: 10.1002/jsfa.10540
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Multivariate optimization of a new LC–MS/MS method for the determination of 156 pesticide residues in milk and dairy products

Abstract: BACKGROUND Pesticides are widely utilized worldwide to control undesirable life forms during the planting procedure in agriculture. But they can pollute the nature and jeopardize human wellbeing. Additionally, on account of high resistance and biological activity; pesticides are able to accumulate in living organs and lead to acute and long‐term negative effects along with toxicity. Milk and dairy products constitute an important part of a humans’ diet since they contain fundamental supplements and nutrients, … Show more

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Cited by 7 publications
(3 citation statements)
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“…This study used acetonitrile with 1% acetate as an extraction solvent because it can extract various compounds with different polarity ranges and is the most effective organic solvent in multi-residue methods [17,18,20]. The volumes of extraction solution, such as 10 mL, 16 mL, and 20 mL of acetonitrile with 1% acetate, were compared to improve the extraction efficiency.…”
Section: Optimization Of the Extraction Solvent Volumementioning
confidence: 99%
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“…This study used acetonitrile with 1% acetate as an extraction solvent because it can extract various compounds with different polarity ranges and is the most effective organic solvent in multi-residue methods [17,18,20]. The volumes of extraction solution, such as 10 mL, 16 mL, and 20 mL of acetonitrile with 1% acetate, were compared to improve the extraction efficiency.…”
Section: Optimization Of the Extraction Solvent Volumementioning
confidence: 99%
“…Therefore, to meet these requirements, there is an increasing need for an effective analytical method for simultaneous qualitative and quantitative screening of pesticide residues in milk. The current reported methods for the analysis of multiresidue pesticides in milk use different detection techniques, such as high-performance liquid chromatography with diode-array detection (HPLC-DAD) [12], gas chromatographyelectron capture detection (GC-ECD) [13], gas chromatography-mass spectrometry (GC-MS) [14], gas chromatography-tandem mass spectrometry (GC-MS/MS) [15,16], and liquid chromatography-tandem mass spectrometry (LC-MS/MS) [17][18][19]. Recently, liquid chromatography coupled with high-resolution mass spectrometry techniques (LC-HRMS) had been applied to determine pesticide residues in milk matrices [20,21].…”
Section: Introductionmentioning
confidence: 99%
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