“…9, the main characteristic bands of polyaniline at 827 cm À1 , 1141 cm À1 , 1301 cm À1 , 1502 cm À1 , 1577 cm À1 could be seen in the FT-IR spectrum, corresponding to CAH vibration out of benzene plane, CAN stretching of ANHA(C 6 H 4 )ANHA, stretching vibration of CAN bond linked with benzenoid ring, benzenoid structure (C@C) and quinoid (C@C, C@N), respectively [45]. However, two new characteristic bands of solid intermediate products appeared at 1416 cm À1 and 1445 cm À1 , attributing to the ring stretching vibrations in a newly formed phenazine segment [46,47]. Therefore, a reasonable mechanism to form the solid intermediate products was speculate (Fig.…”