Natural deep eutectic solvent as a green extraction medium for the ultrasonic-assisted extraction of sinapine thiocyanate from black mustard seeds

Liu, Ziteng; Sun, Tingting; Liu, Jianxiang; Liang, Ning; Zhao, Longshan

doi:10.1016/j.microc.2024.110549

Microchemical Journal

2024

DOI: 10.1016/j.microc.2024.110549

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Natural deep eutectic solvent as a green extraction medium for the ultrasonic-assisted extraction of sinapine thiocyanate from black mustard seeds

Ziteng Liu,

Tingting Sun,

Jianxiang Liu

et al.

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Development of analytical method for determination of 1,3‐dimethylamylamine in sports nutrition and bodybuilding supplements using pH‐switchable deep eutectic solvents followed by high‐performance liquid chromatography‐diode array detector

Shen,

Zhang,

Zhang

et al. 2024

J of Separation Science

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In this work, an easy, safe, simple, and efficient pH‐switchable deep eutectic solvents (DESs)‐based liquid phase microextraction followed by high‐performance liquid chromatography‐diode array detector analysis was developed for the determination of 1,3‐dimethylamylamine (DMAA). The switchability of the obtained DESs was investigated by changing the pH. Then the best‐selected DES was characterized and the application of the selected DES in the extraction of DMAA from sports nutrition and bodybuilding supplements was investigated. The DES synthesized from l‐menthol: oleic acid in a molar ratio of 1:2 had the highest efficiency in the extraction of the target compound. Under the optimum conditions, (50 µL of DES, 100 µL of 4 mol/L KOH, 100 µL of 4 mol/L HCl, extraction time of 40 s and without salt addition) the calibration graph was linear in the range of 0.05–100 µg/kg and limit of detection was 0.02 µg/kg. The relative standard deviations including intra‐day and inter‐day for 10.0 µg/kg of DMAA in real samples were 2.7% (n = 7) and 5.3% (n = 7), respectively. The enrichment factor and percentage extraction recovery of the method were 283 and 85%, respectively. The relative recoveries for DMAA in different samples were in the range of 90%–109%.

show abstract

Development of analytical method for determination of 1,3‐dimethylamylamine in sports nutrition and bodybuilding supplements using pH‐switchable deep eutectic solvents followed by high‐performance liquid chromatography‐diode array detector

Shen,

Zhang,

Zhang

et al. 2024

J of Separation Science

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Choline chloride-based solvents as alternative media for alginate extraction from brown seaweed

Hiemstra,

Meinema,

Eppink

et al. 2024

LWT

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A phospho-modified hyper crosslinked polymer as adsorbent for high-efficiency enrichment of phenols from food samples

Jing,

Ma,

Liu

et al. 2025

Microchemical Journal

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Natural deep eutectic solvent as a green extraction medium for the ultrasonic-assisted extraction of sinapine thiocyanate from black mustard seeds

Cited by 3 publications

References 44 publications

Development of analytical method for determination of 1,3‐dimethylamylamine in sports nutrition and bodybuilding supplements using pH‐switchable deep eutectic solvents followed by high‐performance liquid chromatography‐diode array detector

Development of analytical method for determination of 1,3‐dimethylamylamine in sports nutrition and bodybuilding supplements using pH‐switchable deep eutectic solvents followed by high‐performance liquid chromatography‐diode array detector

Choline chloride-based solvents as alternative media for alginate extraction from brown seaweed

A phospho-modified hyper crosslinked polymer as adsorbent for high-efficiency enrichment of phenols from food samples

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