New Trend in the Extraction of Pesticides from the Environmental and Food Samples Applying Microextraction Based Green Chemistry Scenario: A Review

Jagirani, Muhammad Saqaf; Özalp, Özgür; Soylak, Mustafa

doi:10.1080/10408347.2021.1874867

Cited by 37 publications

(8 citation statements)

References 287 publications

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“…However, they have been implemented less or not at all in routine laboratories for the control of pesticide residues. In general, the main objective of these approaches has been to decrease the solvent consumption, which has led to the miniaturization of traditional sample treatments [83]. Solid-phase microextraction (SPME) is the most popular of these microextraction techniques, and involves the extraction of target analytes with a thin fiber made of fused silica coated with a suitable stationary phase.…”

Section: Chromatographic Separations In Ms-based Methodsmentioning

confidence: 99%

Current Role of Mass Spectrometry in the Determination of Pesticide Residues in Food

Hernández‐Mesa

Moreno‐González

2022

Separations

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The extensive use of pesticides represents a risk to human health. Consequently, legal frameworks have been established to ensure food safety, including control programs for pesticide residues. In this context, the performance of analytical methods acquires special relevance. Such methods are expected to be able to determine the largest number of compounds at trace concentration levels in complex food matrices, which represents a great analytical challenge. Technical advances in mass spectrometry (MS) have led to the development of more efficient analytical methods for the determination of pesticides. This review provides an overview of current analytical strategies applied in pesticide analysis, with a special focus on MS methods. Current targeted MS methods allow the simultaneous determination of hundreds of pesticides, whereas non-targeted MS methods are now applicable to the identification of pesticide metabolites and transformation products. New trends in pesticide analysis are also presented, including approaches for the simultaneous determination of pesticide residues and other food contaminants (i.e., mega-methods), or the recent application of techniques such as ion mobility–mass spectrometry (IM–MS) for this purpose.

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Section: Chromatographic Separations In Ms-based Methodsmentioning

confidence: 99%

Current Role of Mass Spectrometry in the Determination of Pesticide Residues in Food

Hernández‐Mesa

Moreno‐González

2022

Separations

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“…Over the years, a number of conventional techniques have been developed to extract different types of contaminants from environments. Pesticides, PAHs, PCBs, pharmaceuticals, and others are extracted from the environment using a variety of techniques, such as microwave extraction, ultrasonic extraction, and Soxhlet extraction [ 142 , 143 , 144 ]. However, low extraction efficiency, large organic solvent consumption, low reproducibility, extended extraction duration, and solvent diffusion are some of their drawbacks.…”

Section: Types Of Analytes Extractedmentioning

confidence: 99%

A Review: Subcritical Water Extraction of Organic Pollutants from Environmental Matrices

Yabalak,

Aminzai,

Gizir

et al. 2024

Molecules

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Most organic pollutants are serious environmental concerns globally due to their resistance to biological, chemical, and photolytic degradation. The vast array of uses of organic compounds in daily life causes a massive annual release of these substances into the air, water, and soil. Typical examples of these substances include pesticides, polychlorinated biphenyls (PCBs), and polycyclic aromatic hydrocarbons (PAHs). Since they are persistent and hazardous in the environment, as well as bio-accumulative, sensitive and efficient extraction and detection techniques are required to estimate the level of pollution and assess the ecological consequences. A wide variety of extraction methods, including pressurized liquid extraction, microwave-assisted extraction, supercritical fluid extraction, and subcritical water extraction, have been recently used for the extraction of organic pollutants from the environment. However, subcritical water has proven to be the most effective approach for the extraction of a wide range of organic pollutants from the environment. In this review article, we provide a brief overview of the subcritical water extraction technique and its application to the extraction of PAHs, PCBs, pesticides, pharmaceuticals, and others form environmental matrices. Furthermore, we briefly discuss the influence of key extraction parameters, such as extraction time, pressure, and temperature, on extraction efficiency and recovery.

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“…The selection of configurations can be tailored to a particular objective, considering their respective benefits and drawbacks. One of the benefits of SPME is its solvent-free nature, making it a more environmentally friendly option [ 23 ].…”

Section: Microextraction Techniquesmentioning

confidence: 99%

Arsenic speciation by using emerging sample preparation techniques: a review

JAGIRANI,

SOYLAK

2023

Turkish Journal of Chemistry

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Arsenic is a hazardous element that causes environmental pollution. Due to its toxicological effects, it is crucial to quantify and minimize the hazardous impact on the ecology. Despite the significant advances in analytical techniques, sample preparation is still crucial for determining target analytes in complex matrices. Several factors affect the direct analysis, such as trace-level analysis, advanced regulatory requirements, complexity of sample matrices, and incompatible with analytical instrumentation. Along with the development in the sample preparation process, microextraction methods play an essential role in the sample preparation process. Microextraction techniques (METs) are the newest green approach that replaces traditional sample preparation and preconcentration methods. METs have minimized the limitation of conventional sample preparation methods while keeping all their benefits. METs improve extraction efficacy, are fast, automated, use less amount of solvents, and are suitable for the environment. Microextraction techniques with less solvent consumption, such as solid phase microextraction (SPME) solvent-free methods, and liquid phase microextraction (LPME), are widely used in modern analytical procedures. SPME development focuses on synthesizing new sorbents and applying online sample preparation, whereas LPME research investigates the utilization of new solvents.

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New Trend in the Extraction of Pesticides from the Environmental and Food Samples Applying Microextraction Based Green Chemistry Scenario: A Review

Cited by 37 publications

References 287 publications

Current Role of Mass Spectrometry in the Determination of Pesticide Residues in Food

Current Role of Mass Spectrometry in the Determination of Pesticide Residues in Food

A Review: Subcritical Water Extraction of Organic Pollutants from Environmental Matrices

Arsenic speciation by using emerging sample preparation techniques: a review

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