Abstract:The authors conducted free radical polymerization using an initiator to synthesize a copolymer of isobornyl methacrylate—Acrylonitrile (I/A). The reactivity ratios of I (r1) and A (r2) monomers were determined as r1 = 1.63 ± 0.14, r2 = 0.61 ± 0.06 for linear KT (Kelen–Tudos) method and r1 = 1.58, r2 = 0.60 for the EVM (Error-in-Variable Method). We interpreted 1H and 13C{1H} NMR spectra of the I/A copolymers using DEPT-135 and 2D HSQC spectra. The α-CH3 carbon in the I-unit was identified and confirmed using a… Show more
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