Optical setup for a piston-cylinder type pressure cell: a double-volume approach

Abstract

Measurement of the absolute value of the applied pressure in high-pressure muon and neutron experiments is a complicated task. It requires both the presence of a calibration material inside the sample volume as well as additional time for refining the response of the calibrant. Here we describe the use of optical calibrants for precise determination of the pressure value inside the piston-cylinder clamp cells. Utilizing the concept of separate volumes for the sample and the optical media, a new setup for conducting in-situ pressure measurements has been successfully tested. Pressures in both the 'sample' and the 'optical' volumes were proved to be the same within experimental accuracy. The use of SrB4O7:(0.01 Sm 2+ , 0.03 Eu 2+ ) as a pressure calibrant allows for a high accuracy of pressure determination by considering up to eight fluorescence lines.