Optimization of microwave assisted extraction of pectin from orange peel

Maran, J. Prakash; Sivakumar, V.; Thirugnanasambandham, K.; Sridhar, R.

doi:10.1016/j.carbpol.2013.05.052

Cited by 278 publications

(102 citation statements)

References 20 publications

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“…Finally, the pectin yield was 0.037 and 0.18 kg of pectin per kg of fresh orange peel and dry orange peel respectively. The yield on dry basis is similar to other obtained with other techniques such as 0.19 with microwave-assisted extraction and 0.18 with a high hydrostatic pressure treatment [28,29]. These results suggests that orange peel can be used as raw material to obtain D-limonene as an intermediate compound and produce other important products reaching an integrated utilization of orange peel [30].…”

Section: Resultssupporting

confidence: 72%

Techno-economic and Environmental Assessment of p-Cymene and Pectin Production from Orange Peel

Dávila

Rosenberg

Cardona

2015

Waste Biomass Valor

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Citrus production generates a large quantities of residues which can be used in the production of intermediate compounds for the production of value added products which can be used in the synthesis of industrial fine chemicals, fragrances, flavorings, herbicides, pharmaceutical products among others. This work presents a study to increase the value added of essential oils obtained from orange peel producing pcymene and pectin. Techno-economic and environmental assessments were developed demonstrating that computeraided process engineering tools can be used to evaluate the feasibility of integrated processes. Two scenarios were evaluated (with and without electricity generation) obtaining 9.22 and 42.63 kg/h with purities of 97 and 81 % of p-cymene and pectin respectively. In the scenario with electricity generation, 99.81 kWh was obtained, covering all requirements in the process. The techno-economic analysis showed that the most appropriate scheme was that without electricity generation reaching a production cost of 5.27 and 3.53 USD/kg of pcymene and pectin respectively. Environmental analysis reveals that the potential environmental impact was lowest for the scenario without electricity generation.

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Section: Resultssupporting

confidence: 72%

Techno-economic and Environmental Assessment of p-Cymene and Pectin Production from Orange Peel

Dávila

Rosenberg

Cardona

2015

Waste Biomass Valor

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“…The 3 D plot between the irradiation power (X 1 ) and solvent per g of drug (X 3 ) for 325 sec (mid level) established the relationship independent variable (X 3 ) and dependent variable (R) (Figure 6(c)). The observation of plot reveals the linear rise of marrubiin yield with solvent concentration upto 30 mL/g of drug, because the optimum amount of solvent breaks the mass transfer barrier and promotes the movement of plant actives out of the cell matrix (Prakash Maran et al 2013b).…”

Section: Response Surface Analysismentioning

confidence: 99%

Intensification of marrubiin concentration by optimization of microwave-assisted (low CO ₂ yielding) extraction process for Marrubium vulgare using central composite design and antioxidant evaluation

Mittal

Nanda

2017

Pharmaceutical Biology

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Context: Marrubium vulgare Linn (Lamiaceae) was generally extracted by conventional methods with low yield of marrubiin; these processes were not considered environment friendly. Objective: This study extracts the whole plant of M. vulgare by microwave assisted extraction (MAE) and optimizes the effect of various extraction parameters on the marrubiin yield by using Central Composite Design (CCD). Materials and methods: The selected medicinal plant was extracted using ethanol: water (1:1) as solvent by MAE. The plant material was also extracted using a Soxhlet and the various extracts were analyzed by HPTLC to quantify the marrubiin concentration. Results: The optimized conditions for the microwave-assisted extraction of selected medicinal plant was microwave power of 539 W, irradiation time of 373 s and solvent to drug ratio, 32 mL per g of the drug. The marrubiin concentration in MAE almost doubled relative to the traditional method (0.69 ± 0.08 to 1.35 ± 0.04%). The IC 50 for DPPH was reduced to 66.28 ± 0.6 lg/mL as compared to conventional extract (84.14 ± 0.7 lg/mL). The scanning electron micrographs of the treated and untreated drug samples further support the results. Discussion and conclusion: The CCD can be successfully applied to optimize the extraction parameters (MAE) for M. vulgare. Moreover, in terms of environmental impact, the MAE technique could be assumed as a 'Green approach' because the MAE approach for extraction of plant released only 92.3 g of CO 2 as compared to 3207.6 g CO 2 using the Soxhlet method of extraction. ARTICLE HISTORY

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“…Moreover, RSM has been widely used for optimization of various wastewater treatment processes. 7 The results obtained from this study will useful to bagasse based paper and pulp industry wastewater treatment plants (WTP) for treating their effluents in a very effective manner with resanoable operating cost.…”

Section: Introductionmentioning

confidence: 99%

Analysis of Efficiency of Bacillus subtilis To Treat Bagasse Based Paper and Pulp Industry Wastewater-A Novel Approach

Karichappan¹,

Venkatachalam²,

Maran³

2014

Journal of the Korean Chemical Society

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In this present study, bagasse based pulp and paper industry wastewater was treated under different operating conditions such as initial pH (6-8), temperature (25-35 o C) and contact time (3-7 days) by using Bacillus subtilis. Response surface methodology (RSM) coupled with Box-Behnken response surface design (BBD) was employed to investigate the effect of process variables on the responses such as turbidity, biological oxygen demand (BOD) and chemical oxygen demand (COD) removal. The experimental data were analyzed by Pareto analysis of variance (ANOVA) and the second order polynomial models were developed. Interactive effects of the process variables on the responses were studied using plotting 3D response surface contour graph and the optimum process conditions were found to be: initial pH of 7, temperature of 30 o C and contact time of 5 days. Under these conditions, removal efficiencies of turbidity, BOD and COD were found to be 85%, 93% and 80% respectively which are close agreement with real experiments. These results indicate that the treatment of bagasse based pulp and paper industry wastewater using Bacillus subtilis is an effective and novel technique.

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Optimization of microwave assisted extraction of pectin from orange peel

Cited by 278 publications

References 20 publications

Techno-economic and Environmental Assessment of p-Cymene and Pectin Production from Orange Peel

Techno-economic and Environmental Assessment of p-Cymene and Pectin Production from Orange Peel

Intensification of marrubiin concentration by optimization of microwave-assisted (low CO ₂ yielding) extraction process for Marrubium vulgare using central composite design and antioxidant evaluation

Analysis of Efficiency of Bacillus subtilis To Treat Bagasse Based Paper and Pulp Industry Wastewater-A Novel Approach

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Optimization of microwave assisted extraction of pectin from orange peel

Cited by 278 publications

References 20 publications

Techno-economic and Environmental Assessment of p-Cymene and Pectin Production from Orange Peel

Techno-economic and Environmental Assessment of p-Cymene and Pectin Production from Orange Peel

Intensification of marrubiin concentration by optimization of microwave-assisted (low CO 2 yielding) extraction process for Marrubium vulgare using central composite design and antioxidant evaluation

Analysis of Efficiency of Bacillus subtilis To Treat Bagasse Based Paper and Pulp Industry Wastewater-A Novel Approach

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Intensification of marrubiin concentration by optimization of microwave-assisted (low CO ₂ yielding) extraction process for Marrubium vulgare using central composite design and antioxidant evaluation