“…The mixture was stirred for 3 hours. The liberated diborane was collected by a trap in a liquid nitrogen bath, or absorbed by acetone for chemical analysis [13] in 94% yield based both on H and on B.…”
Section: Reaction Of Boraize-triethylamiize Complex With Alumilium Trmentioning
“…The mixture was stirred for 3 hours. The liberated diborane was collected by a trap in a liquid nitrogen bath, or absorbed by acetone for chemical analysis [13] in 94% yield based both on H and on B.…”
Section: Reaction Of Boraize-triethylamiize Complex With Alumilium Trmentioning
“…2-Oxaadamantane has previously been synthesized in a number of other ways. [7][8][9][10][11][12][13][14][15][16] Compound 4 could be transformed into oxalate 5, but attempted reduction with tributyltin hydride gave back hemiacetal 4 (Scheme 2).…”
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.