Physical Characterization and Rheological Behavior of AA 2017 Powder Modified with Al-5.0Nb-0.5B Inoculant Powder for Laser-based Powder Bed Fusion

Abstract

Blending finer powders of Ti, Zr, Ta, Sc, and Nb compounds as inoculants have been a promising strategy to modify precipitation-hardened aluminum alloys for laser-based powder bed fusion, promoting a crack-free equiaxed microstructure. However, there is still a lack of comprehensive understanding of the influence of these fine Al-Nb-B inoculant particles on the AA 2017 powder's physical characteristics and flowability during the process. The results indicate that blended powder has a similar PSD to AA 2017 powder. Furthermore, the circularity, smoothness, and morphology of the particles indicate that both inoculant and AA2017 powders do not exhibit high sphericity, but the blended powder showed slightly more agglomerated particles. Regarding rheological properties, it was observed that a higher flow energy was required to move the blended powder in unconfined conditions compared to the AA 2017 powder. Additionally, the blended powder exhibited higher compressibility and tendency to retain air in packed conditions during the deposition and spreading process. In conclusion, the physical characterization techniques combined with rheological tests have proven to be a rapid and reliable approach for assessing the impact of the finer inoculant particles' characteristics on the laser-based powder bed fusion.