2015
DOI: 10.1080/00032719.2015.1039016
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Polythiophene–Clay Composite Solid-Phase Microextraction Fiber: Preparation, Characterization, and Application to the Determination of Methanol in Biodiesel

Abstract: A novel polymer-clay composite solid phase microextraction fiber is reported for the adsorption of methanol in biodiesel with subsequent determination by gas chromatography coupled with a flame ionization detector. The fiber was fabricated using a stainless steel wire that was subjected to electropolymerization in 0.1 molar NaClO4 containing thiophene and montmorillonite clay dispersed in acetonitrile. Electrochemical deposition was maintained by cycling the potential from 0.2 to 2.2 volts at a scan rate of … Show more

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