2016
DOI: 10.1016/j.dental.2015.12.003
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Probing the dual function of a novel tertiary amine compound in dentin adhesive formulations

Abstract: Objectives A novel tertiary amine compound containing three methacrylate-urethane groups was synthesized for application in dentin adhesives. The synthesis, photopolymerization kinetics, and leaching were examined in an earlier study using this novel compound as the co-initiator (0.5 and 1.75 wt% based on the total resin mass). The objective of this work was to investigate the potential of TUMA (8-(2-(((2-(methacryloyloxy)ethyl)carbamoyl)oxy)propyl)-6,10-dimethyl-4,12-dioxo-5,11-dioxa-3,8,13-triazapentadecane-… Show more

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Cited by 11 publications
(14 citation statements)
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“…In our previous study, amine-functionalized co-monomers have been introduced into the dental adhesive resin and the copolymers showed a long-term neutralization capacity [34,53,63,64]. In the present work, with the incorporation of amine functionalized poly-merizable component (SNM), the copolymers showed promising neutralization capacity, which could offer the benefit of maintaining the neutral pH at the localized micro-environment of the restorative material/tooth interface.…”
Section: Discussionmentioning
confidence: 71%
“…In our previous study, amine-functionalized co-monomers have been introduced into the dental adhesive resin and the copolymers showed a long-term neutralization capacity [34,53,63,64]. In the present work, with the incorporation of amine functionalized poly-merizable component (SNM), the copolymers showed promising neutralization capacity, which could offer the benefit of maintaining the neutral pH at the localized micro-environment of the restorative material/tooth interface.…”
Section: Discussionmentioning
confidence: 71%
“…The preparation of the adhesive formulations has been reported [1517]. There are two experimental adhesive formulations with 2.5 and 5.0 wt % of lysine, respectively.…”
Section: Methodsmentioning
confidence: 99%
“…The preparation of the round-beam shaped polymer specimens for dynamic mechanical analysis and thermogravimetric analysis has been reported previously [17]. In brief, resin was first injected into glass-tubing molds with a diameter of 1 mm (Fiber Optic Center, Inc., part no.…”
Section: Methodsmentioning
confidence: 99%
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