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“…A useful laboratory reaction is the oxidation of malonic ester with nitrogen trioxide (33,34,35,36,74,194) or nitrogen tetroxide (73) oxomalonate. The reagents are mixed while cold and allowed to warm gradually to room temperature, and the product is distilled.…”
Section: Reactions With Compounds Containing Active Methylene Groupsmentioning
confidence: 99%
“…A useful laboratory reaction is the oxidation of malonic ester with nitrogen trioxide (33,34,35,36,74,194) or nitrogen tetroxide (73) oxomalonate. The reagents are mixed while cold and allowed to warm gradually to room temperature, and the product is distilled.…”
Section: Reactions With Compounds Containing Active Methylene Groupsmentioning
confidence: 99%
“…The nitroso or isonitroso compound (XI) is generally believed to be the main by-product which tends to decompose upon distillation. (36) believed that XII was formed during the reaction, and possibly ethyl dinitroacetate also.…”
Section: Reactions With Compounds Containing Active Methylene Groupsmentioning
confidence: 99%
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