2024
DOI: 10.1002/jrs.6743
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Raman Thermometry for Temperature Assessment of Inorganic Transformations During Microwave Heating

John Jamboretz,
Christina S. Birkel

Abstract: Microwave heating is an intriguing method for the synthesis of inorganic solids offering a variety of advantages over conventional furnace heating, such as fast heating and cooling rates as well as volumetric and selective heating of precursors. However, there are many open questions regarding this “black‐box” process, and insights into the effect of microwave radiation on different types of solids are generally missing. In situ Raman spectroscopy is a powerful technique to unravel chemical transformations and… Show more

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