“…13 C NMR (100 MHz, CDCl 3 ) d 182. 88, 155.49, 142.33, 142.06, 137.71, 131.18, 124.19, 123.45, 121.33, 118.20, 107.10, 77.48, 77.16, 76.84, 47.78, 38.00, 31.95, 30.05, 29.75, 29.65, 29.40, 26.64, 22.76, 14.24, 14.20 2,2 0 -(9,9-Didodecyl-9H-fluorene-2,7-diyl) dithiophene (9). In a two-necked round bottom flask, a mixture of 2,7-dibromo-9,9-didodecyl-9H-fluorene (8) (1.51 mmol, 1 g), 2-tributylstannylthiophene (4.5 mmol, 1.69 g) and Pd(PPh 3 ) 4 (0.151 mmol, 174 mg) in anhydrous toluene (30 mL) was taken.…”