2016
DOI: 10.1016/j.chroma.2015.12.021
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Screening and confirmatory method for multiclass determination of 62 antibiotics in meat

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Cited by 47 publications
(43 citation statements)
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“…The mean recoveries were in the interval from 70 to 120%, except for sulfaguanidine, sulfapyridine and sulfamethazine with recoveries from 60 to 70% Although all intra‐lab reproducibilities were lower than or equal to 22%, these three sulfonamides, together with cloxacillin and tylvalosin, demonstrated also the poorest intra‐lab reproducibility (CV wR,pooled >15%). Good recoveries were observed also for beta‐lactams and tetracyclines that demonstrated the most critical performances in muscle tissue . It must be underlined that these performance characteristics were obtained applying the screening run parameters (Table ).…”
Section: Resultsmentioning
confidence: 83%
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“…The mean recoveries were in the interval from 70 to 120%, except for sulfaguanidine, sulfapyridine and sulfamethazine with recoveries from 60 to 70% Although all intra‐lab reproducibilities were lower than or equal to 22%, these three sulfonamides, together with cloxacillin and tylvalosin, demonstrated also the poorest intra‐lab reproducibility (CV wR,pooled >15%). Good recoveries were observed also for beta‐lactams and tetracyclines that demonstrated the most critical performances in muscle tissue . It must be underlined that these performance characteristics were obtained applying the screening run parameters (Table ).…”
Section: Resultsmentioning
confidence: 83%
“…The chromatographic conditions were the same described in our previous paper developed for a multiclass method for antibiotics in muscle . In contrast, important changes have been carried out in MS conditions for milk considering the stringent MRLs especially for some penicillins (4 µg kg −1 ) and specific matrix interfering substances as detailed in the following discussion.…”
Section: Resultsmentioning
confidence: 99%
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