2007
DOI: 10.1016/j.chroma.2006.12.064
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Simultaneous determination of multi-component mycotoxin contaminants in foods and feeds by ultra-performance liquid chromatography tandem mass spectrometry

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Cited by 220 publications
(145 citation statements)
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“…Special attention was paid to the selection of proper eluents, the chromatographic column, and MS/MS conditions to achieve the highest possible sensitivity. The LOQs below 0.01 μg/kg for AFs, low intraday and interday precision (RSD below 10%), and high recoveries (70-110%) (see the electronic supplementary material) achieved passed the criteria of the official methods for mycotoxin determination in baby food [40].…”
Section: Solid-phase Extractionmentioning
confidence: 99%
See 1 more Smart Citation
“…Special attention was paid to the selection of proper eluents, the chromatographic column, and MS/MS conditions to achieve the highest possible sensitivity. The LOQs below 0.01 μg/kg for AFs, low intraday and interday precision (RSD below 10%), and high recoveries (70-110%) (see the electronic supplementary material) achieved passed the criteria of the official methods for mycotoxin determination in baby food [40].…”
Section: Solid-phase Extractionmentioning
confidence: 99%
“…The method performance characteristics summarized in the electronic supplementary material show that because of MycoSep-based purification, low LODs can be achieved without highly sensitive stateof-the-art LC-MS/MS systems having to be used. An in-house validation of another method including MycoSep ® 226 was done for 17 mycotoxins, including AFs and trichothecenes, in various foods and feed [40]. Special attention was paid to the selection of proper eluents, the chromatographic column, and MS/MS conditions to achieve the highest possible sensitivity.…”
Section: Solid-phase Extractionmentioning
confidence: 99%
“…Ren et al established an ultra-performance liquid chromatography (UPLC)-MS/MS method that could detect 14 mycotoxins [14]. Jackson et al improved an LC/MS protocol that provided a practical method for large-scale detection and quantification of multiple mycotoxins in animal feed matrices [15].…”
Section: Introductionmentioning
confidence: 99%
“…Hence, the aforementioned conditions (Eqs. [3][4][5][6] are indeed very important. Based on all of these criteria, the best RBFNNs model was obtained for the test set including 17 compounds.…”
Section: Predictive Power Of Rbfnns Qsrr Model (Validation Of Externamentioning
confidence: 99%
“…[3]. Citrinin (a nephrotoxic, cytotoxic, and genotoxic metabolite produced by several Penicillium species and Aspergillus terreus) and gliotoxin (an immunosuppressive, cytotoxic metabolite with antibiotic and antifungal properties produced by several Aspergillus species) [4] due to their frequent occurrence and their severe effects on animal and human health. These mycotoxins represent a diverse range of chemical structures.…”
Section: Introductionmentioning
confidence: 99%