1993
DOI: 10.1088/0953-2048/6/9/005
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Sinter-forged (Bi, Pb)2Sr2Ca2Cu3Oxsuperconductors

Abstract: Dense (Bi, Pb), Sr,Ca,Cu,O, bars were fabricated by sinter forging. The bars were highly phase-pure and exhibited strong textures in which t h e c axes of the platelike grains were preferentially aligned parallel to the pressing direction. Transport critical current densities increased with texture, reaching a maximum of 8 x io3 A cm-2 at 77 K in a seif-field. Optimal processing in air occurred at 845-850 "C.

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Cited by 47 publications
(15 citation statements)
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“…High-quality bulk specimens with high J c ͑Ͼ1000 A/cm 2 at 77 K͒ have been fabricated by sinter forging. 12 Large bars with good mechanical integrity can be easily cut to produce controlled defects. Another advantage is that the BSCCO/Ag bond was fabricated separately, allowing contact resistance to be varied in a separate heat treatment step.…”
Section: A Experimental Proceduresmentioning
confidence: 99%
“…High-quality bulk specimens with high J c ͑Ͼ1000 A/cm 2 at 77 K͒ have been fabricated by sinter forging. 12 Large bars with good mechanical integrity can be easily cut to produce controlled defects. Another advantage is that the BSCCO/Ag bond was fabricated separately, allowing contact resistance to be varied in a separate heat treatment step.…”
Section: A Experimental Proceduresmentioning
confidence: 99%
“…It is recognized that better J c values have been reported for a monolithic BPSCCO material, 41,42 using similar hot-pressing or hot-forging techniques at higher temperatures between 840 and 850 ± C. In this study, the solid-state processing method was developed as a routine technique for fabricating large bulk monolithic BPSCCO and (MgO) w ͞BPSCCO composite specimens with a consistent good quality for subsequent thermomechanical property studies, which are considered to be critical in the new HTS material development. In order to preserve the specimen integrity by minimizing liquid phase formation, the hot pressing was performed at relatively low temperatures up to 820 ± C.…”
Section: Effect Of Repeated Hot Pressing and Annealingmentioning
confidence: 99%
“…Nevertheless, hot forming has proved to be quite successful for fabrication of bulk high-temperature superconductors, so long as deformation rates are low or large hydrostatic stresses are applied. [13][14][15][16][17][18][19][20] Steady-state creep data have proved to be useful in designing optimal heat treatments for superconductors and in support of more-fundamental diffusion experiments. 212-2 The hightemperature superconductors are highly complex oxides, and it is a challenge to understand their deformation responses.…”
Section: I I 1_ I_ _limentioning
confidence: 99%