2011
DOI: 10.4028/www.scientific.net/amr.393-395.947
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Solvothermal Synthesis and Magnetic Properties of Fe<sub>3</sub>O<sub>4</sub> Microspheres

Abstract: We synthesized Fe3O4 microspheres using a solvothermal method and characterized their morphologies, structures, surface property and magnetism by field emission scanning electron microscopy (FE-SEM), powder X-ray diffraction (XRD) patterns, Fourier transform infrared (FTIR) absorption spectra, and vibrating sample magnetometer (VSM). The results showed that the synthesized Fe3O4 microspheres with a tunable size range of ca. 80–200 nm are composed of many Fe3O4 collective nanoparticles. XRD pattern confirmed th… Show more

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“…Magnetite particles were synthesized according to previously published protocols [39,40]. In a typical synthesis process, FeCl 3 •6H 2 O (2.16 g) and CH 3 COONa (6 g) were dissolved in 15mL ethylene glycol.…”
Section: Synthesis Of Fe 3 Omentioning
confidence: 99%
“…Magnetite particles were synthesized according to previously published protocols [39,40]. In a typical synthesis process, FeCl 3 •6H 2 O (2.16 g) and CH 3 COONa (6 g) were dissolved in 15mL ethylene glycol.…”
Section: Synthesis Of Fe 3 Omentioning
confidence: 99%