2020
DOI: 10.1002/xrs.3200
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Spectral X‐ray computed micro tomography: 3‐dimensional chemical imaging

Abstract: We present a new approach to 3‐dimensional chemical imaging based on X‐ray computed micro tomography (CT), which enables the analysis of the internal elemental chemistry. The method uses a conventional laboratory‐based CT scanner equipped with a semiconductor detector (CdTe). Based on the X‐ray absorption spectra, elements in a sample can be distinguished by their specific K‐edge energy. The capabilities and performance of this new approach are illustrated with different experiments, i.e. single pure element p… Show more

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Cited by 19 publications
(15 citation statements)
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“…For example, by comparing a classified image from mineral liberation analysis (MLA) of a cross-section of the sample with the corresponding slice in a CT image, it is possible to determine the range of grey-values that correspond to the phases visible at that cross-section [14,23,26]. This validation method will be exemplified for the samples named Carbonate and Sheelite ore. New CT techniques that allow the measurement of chemical information about the elements inside a sample are currently under development, e.g., spectral CT [26,38] or hyperspectral CT [39]. Such methods have the advantage of not requiring sample preparation nor the complex image processing associated with correlative methods.…”
Section: Mineralogical Validationmentioning
confidence: 99%
See 1 more Smart Citation
“…For example, by comparing a classified image from mineral liberation analysis (MLA) of a cross-section of the sample with the corresponding slice in a CT image, it is possible to determine the range of grey-values that correspond to the phases visible at that cross-section [14,23,26]. This validation method will be exemplified for the samples named Carbonate and Sheelite ore. New CT techniques that allow the measurement of chemical information about the elements inside a sample are currently under development, e.g., spectral CT [26,38] or hyperspectral CT [39]. Such methods have the advantage of not requiring sample preparation nor the complex image processing associated with correlative methods.…”
Section: Mineralogical Validationmentioning
confidence: 99%
“…The reconstructed CT value interval was [0, 26]. Using these scanning conditions, the effective energy was calculated from the measured transmission spectrum (Figure S2) using a spectral detector [38]. Image processing was achieved using Avizo.…”
Section: Qz/py Samplementioning
confidence: 99%
“…The main advantage of the spectral content in the images is the possibility of material identification at lab X-ray sources. Due to their construction as full-field pixellated devices, these cameras allow for capture of chemical information not only in X-ray fluorescence (XRF) applications, but also in full-field transmission imaging [ 1 , 2 ] and transmission computed tomography (CT) [ 3 , 4 , 5 ]. Even in the established application domain of XRF imaging, these hyperspectral systems provide added value through their 2D nature as opposed to the single-element energy dispersive detectors commonly used in XRF measurement setups, allowing for improvements in speed and image quality for fluorescence measurements as well [ 6 , 7 , 8 ].…”
Section: Introductionmentioning
confidence: 99%
“…Therefore, chemically different particles can be distinguished inside a sample from a single CT scan. The method is able to distinguish elements with K-edges in the range from 25 to 160 keV, which applies to elements with Z > 48 (Sittner et al, 2020).…”
mentioning
confidence: 99%