Studies on Reactions Relating to Carbohydrates and Polysaccharides. Xxii. The Isomeric Cinnamylidene Glycerols

ATRP-based synthesis of a pH-sensitive amphiphilic block polymer and its self-assembled micelles with hollow mesoporous silica as DOX carriers for controlled drug release

“…was synthesized according to the previously reported method. 22 To a mixture of 132 g of cinnamic aldehyde and 92 g of glycerol, 5 drops of 40% sulfuric acid solution were added dropwise and stirred, the reaction system was evacuated, and the mixture was slowly heated to 100 C. The reaction was continued for 30 min until no water was distilled off. It was cooled to room temperature and the reactants gradually solidied.…”