Abstract:Aminoindano and Related Compounds 3-(5-( 3-Acetamidophenyl)-2-tetrazolyl] propionic -2-tetrazolyl]propionic acid (7 g, 0.03 mol) was stirred for 12 hr at room temp in 100 ml of an equivolume mixture of AcaO-AcOH. The pale yellow ppt was reprecipitated from NaHCOs and recrystd from EtOH to give 5 g (61%) of pale yellow crystals, mp 207°.3-[5-(3-Phenylazophenyl)-2-tetrazolyl]propionic Acid (30).-To a solution of 7 g (0.03 mol) of 3-[5-(3-aminophenyl)-2-tetrazolyl]propionic acid in 75 ml of glacial AcOH was added… Show more
Die Umsetzung von Inden (I) mit aus (II) in situ erzeugten Nitriloxiden ergibt (III), aus dem durch Reduktion mit Lithiumaluminiumhydrid und 179. Spaltung die Aminoalkohole (IV) entstehen.
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