Synthesis, characterization and crystal structure of butyl N-(3-chloropropyl)-(2S)-alaninate hydrochloride

Dimitrijevic, P Dejana; Novakovic, B Sladjana; Radic, R Gordana; Jevtić, Verica V.; Menéndez-Taboada, Laura; García-Granda, Santiago; Trifunovic, R Srecko

doi:10.2298/jsc130214054d

JSCS

2013

DOI: 10.2298/jsc130214054d

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Synthesis, characterization and crystal structure of butyl N-(3-chloropropyl)-(2S)-alaninate hydrochloride

P Dejana Dimitrijevic

B Sladjana Novakovic

R Gordana Radic

et al.

Abstract: The synthesis of butyl N-(3-chloropropyl)-(2S)-alaninate hydrochloride is reported here. The compound was characterized by elemental analysis, infrared, and 1 H-and 13 C-NMR spectroscopy. The structure of butyl N-(3-chloropropyl)-(2S)-alaninate hydrochloride was confirmed by single-crystal X-ray analysis.

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2021

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(S)-Alanine ethyl ester tetracyanidoborate, (C₅H₁₂NO)[B(CN)₄]

Peppel¹,

Köckerling²

2021

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The title molecular salt, C5H12NO+·C4BN4 − or (C5H12NO)[B(CN)4], was obtained as single crystals by slow evaporation of a solution of the compound in acetonitrile over several weeks. The asymmetric unit contains two (S)-alanine ethyl ester cations and two tetracyanidoborate anions, which are linked by N—H...N hydrogen bonds. The compound exhibits a relatively low melting point of 110°C and shows a solid–solid phase transition near room temperature (T s–s = 29°C) on the basis of DSC measurements.

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(S)-Alanine ethyl ester tetracyanidoborate, (C₅H₁₂NO)[B(CN)₄]

Peppel¹,

Köckerling²

2021

IUCr Data

View full text Add to dashboard Cite

show abstract

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Synthesis, characterization and crystal structure of butyl N-(3-chloropropyl)-(2S)-alaninate hydrochloride

Cited by 1 publication

References 5 publications

(S)-Alanine ethyl ester tetracyanidoborate, (C₅H₁₂NO)[B(CN)₄]

(S)-Alanine ethyl ester tetracyanidoborate, (C₅H₁₂NO)[B(CN)₄]

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Synthesis, characterization and crystal structure of butyl N-(3-chloropropyl)-(2S)-alaninate hydrochloride

Cited by 1 publication

References 5 publications

(S)-Alanine ethyl ester tetracyanidoborate, (C5H12NO)[B(CN)4]

(S)-Alanine ethyl ester tetracyanidoborate, (C5H12NO)[B(CN)4]

Contact Info

Product

Resources

About

(S)-Alanine ethyl ester tetracyanidoborate, (C₅H₁₂NO)[B(CN)₄]

(S)-Alanine ethyl ester tetracyanidoborate, (C₅H₁₂NO)[B(CN)₄]