2014
DOI: 10.14723/tmrsj.39.451
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Synthesis of titanium dioxide nanoparticles by solvothermal method with polymer gel

Abstract: Highly dispersed and homogeneous titanium dioxide (TiO 2) nanoparticles were synthesized by a solvothermal method with polymer gel. Polymer gel is essential for the highly dispersed and homogeneous nanoparticles. First, polyvinyl alcohol (PVA) was dissolved in water at 70°C and cooled to room temperature. Ammonium citratoperoxotitanate(IV) [(NH 4) 8 [Ti 4 (C 6 H 4 O 7) 4 (O 2) 4 ]・ 8H 2 O] was subsequently added and dissolved in the PVA solution. Next, water was evaporated from the PVA gel using a microwave. T… Show more

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Cited by 6 publications
(2 citation statements)
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“…Oshima et al [73] used the solvothermal method to obtain TiO 2 nanoparticles. Here, a polymer gel was used, which enabled strongly dispersed and homogeneous particles to be obtained.…”
Section: Solvothermal Methodsmentioning
confidence: 99%
“…Oshima et al [73] used the solvothermal method to obtain TiO 2 nanoparticles. Here, a polymer gel was used, which enabled strongly dispersed and homogeneous particles to be obtained.…”
Section: Solvothermal Methodsmentioning
confidence: 99%
“…Synthesis of TiO2 using titanium (IV) isopropoxide (TTIP) precursor through hydrothermal process by Collazza, et al, showed pure crystalline phase of anatase for all conditions of synthesis [37]. Oshima, et al, synthesized TiO2 with polymer gel by solvothermal method [38]. X-ray diffraction (XRD) confirmed presence of anatase TiO2.…”
Section: Synthesis and Characterization Toolsmentioning
confidence: 99%