2023
DOI: 10.1021/acs.cgd.2c01290
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Synthesis, Structural and Theoretical Analyses of C≡N···I Halogen-Bonded Liquid Crystalline Complexes of 4-Cyano-4′-alkoxy Biphenyl Systems

Abstract: A series of 4-cyano-4′-alkoxybiphenyl compounds were synthesized by varying the spacer chain lengths (−CH 2 −) n , where n = 3−10, for the systematic study of a halogen-bonded (XB) complex with 1,4-diiodotetrafluoro benzene. The XB liquid crystalline complexes obtained from the liquid-assisted grinding method were characterized by FTIR, Raman, DSC, and PXRD studies. Further, C�N•••I XB interaction was established by singlecrystal X-ray diffraction analysis. The odd-even analysis has suggested that the even car… Show more

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