1997
DOI: 10.1039/a608599g
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The synthesis and crystal structures of pyridine-2,6-dicarboxamide oxime, C7H9N5O2, and its nickel(II) and copper(II) co-ordination compounds

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Cited by 19 publications
(10 citation statements)
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“…The ligand pyridine-2,6-diamidoxime (L) was prepared as well as [29] by the reaction of an ethanolic solution of 2,6-dicyanopyridine with a neutralized aqueous solution of hydroxylamine hydrochloride . The infrared spectrum of (L) shows the bands at 3482 and 3414 cm -1 absorptions are assigned as the σ (asym) and σ (sym) NH stretching frequencies,…”
Section: Synthesismentioning
confidence: 99%
See 1 more Smart Citation
“…The ligand pyridine-2,6-diamidoxime (L) was prepared as well as [29] by the reaction of an ethanolic solution of 2,6-dicyanopyridine with a neutralized aqueous solution of hydroxylamine hydrochloride . The infrared spectrum of (L) shows the bands at 3482 and 3414 cm -1 absorptions are assigned as the σ (asym) and σ (sym) NH stretching frequencies,…”
Section: Synthesismentioning
confidence: 99%
“…The majority of these amidoximes are aliphatic compounds which form five-membered rings utilizing the diimine moiety, -N=C-C=N-, involving oxime and imine nitrogens as the co-ordination sites with transition-metal atoms [29].…”
Section: Introductionmentioning
confidence: 99%
“…The complex crystallizes in the monoclinic space group P2 1 /n with the unit cell parameters a = 12.824(3)A°, b = 13.799(2)A°, c = 15.441(4)A° and β= 114.691 (19).with four molecules in the unit cell (one per asymmetric unit) . The asymmetric unit, formed by one Mn 2+ metal ion, two crystallographically independent oxime ligands and two perchlorate counter-ion located on general positions.…”
Section: Structurementioning
confidence: 99%
“…The ligand (L) pyridine-2,6-diamidoxime has been prepared as well as [19][20] by the reaction of of 2,6-dicyanopyridine solution with a neutralized aqueous solution of hydroxylamine hydrochloride . The 1 H NMR shifts and the infrared spectum bands are listed in the Experimental section.…”
Section: Synthesismentioning
confidence: 99%
See 1 more Smart Citation