Thermal behavior of Mannich base N,N′-tetra(4-antipyrylmethyl)-1,2 diaminoethane (TAMEN) and its binuclear complexes

Sasca, Viorel; Mosoarca, Elena Maria; Avram, Livia; Tudose, Ramona; Costişor, Otilia

doi:10.1007/s10973-008-9106-z

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“…Presuming that the biological activity may be affected by the number of antipyrine fragments in the ligand molecule, Co(BAMP)(NCS) 2 [23], M 2 (L)X n where L¼BAMP, TAMEN were obtained [24][25][26][27][28][29][30] and for some of them the structure has been resolved [31][32][33][34][35][36]. Both BAMP and TAMEN contain antipyrine fragments disposed symmetrically on each side of the piperazine or ethylenediamine bridge, respectively.…”

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confidence: 99%

Mixed-ligand complexes of iron(II), iron(III), copper(II), and cobalt(II) with pyrazolonic and 2,2′-bipyridine ligands

Tudose

Mosoarca

Simulescu

et al. 2010

Journal of Coordination Chemistry

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New mixed-ligand complexes, [M 2 (BAMP)(bipy) 2 ][MCl 4 ] 2 , M¼Co þ2 (1), Cu þ2 (2), [M 2 (TAMEN)(bipy) 2 ][MCl 4 ] 2 , M¼Fe þ2 (3), Co 2þ (4), and [Fe 2 (TAMEN)(bipy) 2 ][FeCl 6 ] 2 (5), where BAMP and TAMEN stand for the Mannich bases N,N 0 -bis(antipyryl-4-methylene)-piperazine and N,N 0 -tetra(antipyryl-4-methylene)-1,2-ethane-diamine, respectively, have been obtained and characterized by elemental analyses, conductometric and magnetic susceptibility measurements at room temperature, mass spectrometry, UV-Vis, infrared, and mass spectroscopy, and 1 H NMR spectra for the ligands.

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