1996
DOI: 10.1007/bf01982691
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Thermoplastic polymers quality control

Abstract: A technique is proposed for improving the accuracy of the heat of fusion of semierystalline polymers by DSC. The results of three commercially available instruments are compared.

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Cited by 4 publications
(2 citation statements)
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“…The determination of the heat of fusion from the area of the DSC peak can be performed after establishing a baseline to bind the area that is to be integrated. In this work, the derivative curve is used to calculate the onset temperature,6 the departure of the thermal curve from a horizontal baseline.…”
Section: Methodsmentioning
confidence: 99%
“…The determination of the heat of fusion from the area of the DSC peak can be performed after establishing a baseline to bind the area that is to be integrated. In this work, the derivative curve is used to calculate the onset temperature,6 the departure of the thermal curve from a horizontal baseline.…”
Section: Methodsmentioning
confidence: 99%
“…In this work the derivative curve is used to calculate the onset temperature. 4 The morphology of the crystalline phase of the base polymer can be studied by means of the two characteristics properties previously quoted. The crystallinity is related with the size of the crystalline phase, and it is well known that the melting point depends on the crystallite size.…”
Section: Experimental Dsc (Differential Scanning Calorimetry)mentioning
confidence: 99%