1976
DOI: 10.1021/ac60369a022
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Titrations in nonaqueous solvents

Abstract: This review covers approximately the literature reported in Chemical Abstracts over the period January 1974 to December 1975, plus some additions from other sources. As the editors have requested, emphasis is on developments in theory, methodology, and instrumentation, with applications included only insofar as they appear to advance the state-of-the-art or have particular current relevance. The selection of what to include necessarily is a matter of judgment, and so certain areas may not have received the att… Show more

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Cited by 8 publications
(1 citation statement)
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“…Potentiometric titration is the official test method according to the British Pharmacopoeia (2020), European Pharmacopoeia (2020), Japanese Pharmacopoeia (2021) and United States Pharmacopoeia (2022). However, some aspects of this method can be improved, such as: (i) analytical aspects, since the method does not have high selectivity and specificity, involves difficult solubilization for sample preparation of AA assays, and is performed using a non-aqueous solvent (glacial acetic acid), which is strongly influenced by atmospheric CO 2 , H 2 O or O 2 (Kratochvil, 1976); (ii) economic aspects, since in comparison with methods in aqueous media, it requires high consumption of reagents, especially solvents; and (iii) environmental aspects, due to the high generation of waste.…”
Section: Instrumentationmentioning
confidence: 99%
“…Potentiometric titration is the official test method according to the British Pharmacopoeia (2020), European Pharmacopoeia (2020), Japanese Pharmacopoeia (2021) and United States Pharmacopoeia (2022). However, some aspects of this method can be improved, such as: (i) analytical aspects, since the method does not have high selectivity and specificity, involves difficult solubilization for sample preparation of AA assays, and is performed using a non-aqueous solvent (glacial acetic acid), which is strongly influenced by atmospheric CO 2 , H 2 O or O 2 (Kratochvil, 1976); (ii) economic aspects, since in comparison with methods in aqueous media, it requires high consumption of reagents, especially solvents; and (iii) environmental aspects, due to the high generation of waste.…”
Section: Instrumentationmentioning
confidence: 99%