The paper is devoted to researching various post-processing methods that affect surface quality, physical properties, and mechanical properties of laser additively manufactured steel parts. The samples made of two types of anticorrosion steels—20kH13 (DIN 1.4021, X20Cr13, AISI 420) and 12kH18N9T (DIN 1.4541, X10CrNiTi18-10, AISI 321) steels—of martensitic and austenitic class were subjected to cavitation abrasive finishing and vibration tumbling. The roughness parameter Ra was reduced by 4.2 times for the 20kH13 (X20Cr13) sample by cavitation-abrasive finishing when the roughness parameter Ra for 12kH18N9T (X10CrNiTi18-10) sample was reduced by 2.8 times by vibratory tumbling. The factors of cavitation-abrasive finishing were quantitatively evaluated and mathematically supported. The samples after low tempering at 240 °C in air, at 680 °C in oil, and annealing at 760 °C in air were compared with cast samples after quenching at 1030 °C and tempering at 240 °C in air, 680 °C in oil. It was shown that the strength characteristics increased by ~15% for 20kH13 (X20Cr13) steel and ~20% for 12kH18N9T (X10CrNiTi18-10) steel than for traditionally heat-treated cast samples. The wear resistance of 20kH13 (X20Cr13) steel during abrasive wear correlated with measured hardness and decreased with an increase in tempering temperatures.
Thermal conductivities of two benzophenone single crystals have been measured at temperatures from 4.7 to 270 K. The experimental data for both are consistent for temperatures above 15 K. The thermal conductivity of benzophenone can be represented as a sum of two contributions: κ1 + κTA where κ1 is due to the standard phonon mechanisms accepted for ordered crystals and κTA takes into account the heat flow due to intermolecular hopping of thermally activated intramolecular vibrational modes. The thermal activation contribution in unsubstituted benzophenone is substantially smaller when compared to that in any of the two para-bromobenzophenone polymorphs studied previously. Unlike in the 4-bromobenzophenone crystals, the microscopic agent responsible for intramolecular excitation(s) was not determined. The characteristic intramolecular excitation energy was evaluated to be 220 K, about three times less compared to 4-bromobenzophenone.
The paper is devoted to the research of the effect of ultrasonic postprocessing—specifically, the effects of ultrasonic cavitation-abrasive finishing, ultrasonic plastic deformation, and vibration tumbling on surface quality, wear resistance, and the ability of real aircraft parts with complex geometries and with sizes less than and more than 100 mm to work in exploitation conditions. The parts were produced by laser powder bed fusion from two types of anticorrosion steels of austenitic and martensitic grades—20Kh13 (DIN 1.4021, X20Cr13, AISI 420) and 12Kh18N9T (DIN 1.4541, X10CrNiTi18-10, AISI 321). The finishing technologies based on mechanical action—plastic deformation, abrasive wear, and complex mechanolysis showed an effect on reducing the submicron surface roughness, removing the trapped powder granules from the manufactured functional surfaces and their wear resistance. The tests were completed by proving resistance of the produced parts to exploitation conditions—vibration fatigue and corrosion in salt fog. The roughness arithmetic mean deviation Ra was improved by 50–52% after cavitation-abrasive finishing, by 28–30% after ultrasonic plastic deformation, and by 65–70% after vibratory tumbling. The effect on wear resistance is correlated with the improved roughness. The effect of used techniques on resistance to abrasive wear was explained and grounded.
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