For additive manufacturing of metals, selective laser melting can be employed. The microstructure evolution is directly influenced by processing parameters. Employing a high energy laser system, samples made from austenitic stainless steel were manufactured. The microstructure obtained is characterized by an extremely high degree of anisotropy featuring coarse elongated grains and a h001i texture alongside the build direction during processing. Eventually, the anisotropy of the microstructure drastically affects the monotonic properties of the current material. Recently, techniques allowing for additive manufacturing of highly complex components have been gaining significant attention in both industry and academic research. [1][2][3] As no tools are required for processing, small to medium batches can be produced very efficiently. Polymers and metals can be processed depending on the technique employed; for processing of metals, wire-based techniques are available, but techniques employing a powder bed have the higher impact. Electron beam melting and selective laser melting (SLM Ò ), both melting the powder locally accordingly to data provided by a model stemming from computer-aided design, are widely used nowadays. [1][2][3] From the academic point of view, the high degree of design freedom allowing for an extreme lightweight design and the aspect of microstructural design are very attractive. [4,5] The latter aspect is mainly influenced by process-related parameters such as scanning strategy and energy input. As has been shown by Thijs et al. for an aluminum alloy processed by selective laser melting in a very recent paper, the thermal gradient during cooling and the direction of heat flow are key parameters for microstructure evolution and design, respectively.[4] Numerous metals and alloys have been processed by SLM Ò ; aluminum and titanium alloys, nickel-based alloys, and stainless steels have been the subjects of recent work. [1][2][3][4][5][6][7][8] Focusing on materials such as nickel-based alloys and austenitic steels, high-temperature applications are of interest. For such applications, a coarse-grained anisotropic microstructure is highly attractive.[9] The current paper addresses this topic and introduces a highly anisotropic austenitic alloy 316L directly obtained from powder processed by SLM Ò . The conditions for obtaining such kind of microstructure are discussed in light of the processing parameters.The material employed in the current study was facecentered cubic (fcc) 316L stainless steel. The initial powder with a mean particle size of 40 lm was supplied by SLM Solutions GmbH. For fabrication of cubical and tension specimens, a SLM Ò -280 HL selective laser melting system in combination with MTT AutoFab software (Marcam Engineering GmbH) was used. The tensile specimens were built in the z-direction; thus, the loading axis was parallel to the built direction. Two Yttrium fiber lasers are employed in the current SLM Ò system, featuring maximum beam energies of 400 W and 1000 W, respectively. ...
The use of porous titanium-based implant materials for bone contact has been gaining ground in recent years. Selective laser melting (SLM) is a rapid prototyping method by which porous implants with highly defined external dimensions and internal architecture can be produced. The coating of porous implants produced by SLM with ceramic layers based on calcium phosphate (CaP) remains relatively unexplored, as does the doping of such coatings with magnesium (Mg) to promote bone formation. In this study, Mg-doped coatings of the CaP types octacalcium phosphate and hydroxyapatite (HA) were deposited on such porous implants using the pulsed laser deposition method. The coated implants were subsequently implanted in a rabbit femoral defect model for 6 months. Uncoated implants served as a reference material. Bone-implant contact and bone volume in the region of interest were evaluated by histopathological techniques using a tri-chromatographic Masson-Goldner staining method and by microcomputed tomography (µCT) analysis of the volume of interest in the vicinity of implants. Histopathological analysis revealed that all implant types integrated directly with surrounding bone with ingrowth of newly formed bone into the pores of the implants. Biocompatibility of all implant types was demonstrated by the absence of inflammatory infiltration by mononuclear cells (lymphocytes), neutrophils, and eosinophils. No osteoclastic or foreign body reaction was observed in the vicinity of the implants. µCT analysis revealed a significant increase in bone volume for implants coated with Mg-doped HA compared to uncoated implants.
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