2016
DOI: 10.1002/cbdv.201500233
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1‐Acetyl‐3‐[(3R)‐hydroxyfatty acyl]glycerols: Lipid Compounds from Euphrasia rostkoviana Hayne and E. tetraquetra (Bréb.) Arrond.

Abstract: Five homologous acetylated acylglycerols of 3-hydroxyfatty acids (chain lengths C(14) - C(18)), named euphrasianins A - E, were characterized for the first time in Euphrasia rostkoviana Hayne (Orobanchaceae) by gas chromatography/mass spectrometry (GC/MS) and high-performance liquid chromatography/atmospheric pressure chemical ionization-mass spectrometry (HPLC/APCI-MS(n) ). In addition to mass spectrometric data, structures of euphrasianins were verified via a three-step total synthesis of one representative … Show more

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Cited by 5 publications
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“…In brief, crude extracts (3–5 mg) or reference substances (1 mg) were dissolved in DMF (500 μL) and treated with 300 μL of BSTFA at 105 °C for 15 min. Subsequently, 1 μl aliquots of the corresponding solutions were injected into the GC/MS system …”
Section: Methodsmentioning
confidence: 99%
“…In brief, crude extracts (3–5 mg) or reference substances (1 mg) were dissolved in DMF (500 μL) and treated with 300 μL of BSTFA at 105 °C for 15 min. Subsequently, 1 μl aliquots of the corresponding solutions were injected into the GC/MS system …”
Section: Methodsmentioning
confidence: 99%