2-(Methoxymethyl)adamantan-2-yl 2-methylacrylate

Meng, Qingwei; Li, Yueqing; Chen, Pingping; Zhao, Weijie; Yang, Jing

doi:10.1107/s1600536809042639

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2023

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“…Intramolecular interactions between hydrogen atoms from C4 and acrylate carbonyl oxygen (O1) also had similar short contact distances of 2.4−2.6 Å. The bond distance between C1 and C2 at 1.304(4) Å is consistent with typical C�C bond distances of related acrylates 15,16 and is in agreement with IR and NMR data.…”

Section: Introductionsupporting

confidence: 81%

Synthesis, Characterization, and Energetic Properties of Nitrate Ester Acrylate Polymer

Kuehl,

Schmalzer,

Snyder

et al. 2023

ACS Omega

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An energetic nitrate ester acrylate monomer (4) was synthesized in a total yield of 68% and polymerized to form the energetic nitrate ester acrylate polymer (NEAP). Compound 4 is a liquid at room temperature with a melting point of −8.6 °C and NEAP is a solid with a glass-transition temperature of −8.8 °C. Intermediates leading to 4 and NEAP were characterized by high-resolution mass spectrometry, elemental analysis, Fourier transform infrared spectroscopy, and proton and carbon nuclear magnetic resonance spectroscopies (1H and 13C{1H} NMR). Both 4 and NEAP have electrostatic discharge, friction, and impact sensitivities comparable to those of trinitrotoluene, making NEAP a potential candidate for advanced energetic formulations.

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Section: Introductionsupporting

confidence: 81%

Synthesis, Characterization, and Energetic Properties of Nitrate Ester Acrylate Polymer

Kuehl,

Schmalzer,

Snyder

et al. 2023

ACS Omega

View full text Add to dashboard Cite

show abstract

2-(Methoxymethyl)adamantan-2-yl 2-methylacrylate

Abstract: The title compound, C16H24O3, has a cage-type molecular structure and is of interest with respect to its photochemical properties. The structure displays non-classical intermolecular C—H⋯O hydrogen bonding, which links the molecules into a three-dimensional network.

Cited by 1 publication

References 1 publication

Synthesis, Characterization, and Energetic Properties of Nitrate Ester Acrylate Polymer

Synthesis, Characterization, and Energetic Properties of Nitrate Ester Acrylate Polymer

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2-(Methoxymethyl)adamantan-2-yl 2-methylacrylate

Abstract: The title compound, C16H24O3, has a cage-type mol­ecular structure and is of inter­est with respect to its photochemical properties. The structure displays non-classical inter­molecular C—H⋯O hydrogen bonding, which links the mol­ecules into a three-dimensional network.

Cited by 1 publication

References 1 publication

Synthesis, Characterization, and Energetic Properties of Nitrate Ester Acrylate Polymer

Synthesis, Characterization, and Energetic Properties of Nitrate Ester Acrylate Polymer

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Product

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About

Abstract: The title compound, C16H24O3, has a cage-type molecular structure and is of interest with respect to its photochemical properties. The structure displays non-classical intermolecular C—H⋯O hydrogen bonding, which links the molecules into a three-dimensional network.