Russ Chem Bull
 2010
DOI: 10.1007/s11172-010-0335-5
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3-Ethoxy-2,2-bis(methoxy-NNO-azoxy)propan-1-ol. Synthesis and X-ray diffraction analysis

I. N. Zyuzin
1
,
Н. И. Головина
2
,
Д. Б. Лемперт
3
et al.

Abstract: Reaction of bis(methoxy NNO azoxy)methane with formaldehyde in ethanol gives 3 ethoxy 2,2 bis(methoxy NNO azoxy)propan 1 ol as a minor product along with target 2,2 bis(methoxy NNO azoxy)ethanol. The structure of the former was confirmed by the counter synthesis and X ray diffraction analysis.

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