337. Reactions of αβ-unsaturated cyclic aldehydes and ketones. Part III. The reduction of cryptone. cis- and trans-Dihydrocyptol

Macbeth, A. Killen; Swanson, T. B.

doi:10.1039/jr9380001820

J. Chem. Soc.

1938

DOI: 10.1039/jr9380001820

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337. Reactions of αβ-unsaturated cyclic aldehydes and ketones. Part III. The reduction of cryptone. cis- and trans-Dihydrocyptol

A. Killen Macbeth¹,

T. B. Swanson²

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2011

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The D iels‐ A lder Reaction with Maleic Anhydride*Present address, University of Southern California, Los Angeles, California.

Kloetzel

2011

Organic Reactions

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Analysis of a simple NMR spectrum is fairly easy and straight forward for undergraduate students but analyzing a fairly complex NMR can be very daunting and requires a methodical approach. This work uses the ubiquitous Diels-Alder reaction of methylcyclopentadiene and maleic anhydride to introduce students to an NMR spectrum that consist of inseparable mixtures of isomers and their analysis using advanced NMR spectroscopic techniques. This laboratory experiment further outlines the use of derivatization techniques for the separation of isomeric mixtures by preparing diastereomers and using NMR spectroscopy for their identification.

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The D iels‐ A lder Reaction with Maleic Anhydride*Present address, University of Southern California, Los Angeles, California.

Kloetzel

2011

Organic Reactions

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scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.

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337. Reactions of αβ-unsaturated cyclic aldehydes and ketones. Part III. The reduction of cryptone. cis- and trans-Dihydrocyptol

Cited by 1 publication

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The D iels‐ A lder Reaction with Maleic Anhydride*Present address, University of Southern California, Los Angeles, California.

The D iels‐ A lder Reaction with Maleic Anhydride*Present address, University of Southern California, Los Angeles, California.

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