Abstract:The metals U(VI) and Pd (II) gives yellow coloration with the reagent 4-Hydroxy benzaldehyde thiosemicarbazone(4-HBTS) in acidic medium simultaneous determination of both the metal ions U(VI) and Pd (II) can be done by using second order derivative spectrophotometric technique. For the determination of composition of metal complexes Job's method and mole ratio method were employed.
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