2002
DOI: 10.1023/a:1021302405128
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Cited by 132 publications
(33 citation statements)
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“…Next, the residues was dissolved with hydrochloric acid, filtered and diluted with deionized water. Finally, the concentrations of the metals (Cu, Zn, Pb, Cr, Cd, and Ni) of diluted solution were determined by flame atomic absorption spectrometry (AAS, Solaar-MK II-M6, Thermo Elemental, Fisher Scientific Inc. Toronto, ON, USA) [25,26]. Each soil sample was measured in triplicate and every step of measurements was optimized to meet the quality control standards.…”
Section: Methodsmentioning
confidence: 99%
“…Next, the residues was dissolved with hydrochloric acid, filtered and diluted with deionized water. Finally, the concentrations of the metals (Cu, Zn, Pb, Cr, Cd, and Ni) of diluted solution were determined by flame atomic absorption spectrometry (AAS, Solaar-MK II-M6, Thermo Elemental, Fisher Scientific Inc. Toronto, ON, USA) [25,26]. Each soil sample was measured in triplicate and every step of measurements was optimized to meet the quality control standards.…”
Section: Methodsmentioning
confidence: 99%
“…19 Os extratos obtidos pela digestão nítrico-perclórica (DNP) apresentaram coloração transparente, sem sinais visíveis de material residual, para todos os resíduos estudados. Em alguns casos, como na digestão do material húmico, substrato orgânico e composto orgâni-co, foi necessário adicionar mais 4 mL de ácido nítrico, além dos 6 mL iniciais, para uma digestão completa da matriz orgânica.…”
Section: Resultsunclassified
“…10 Entretanto, pouco se conhece sobre a recuperação relativa de elementos a partir de compostos orgânicos por vários méto-dos de digestão. 3 Daí, a importância de se testar diferentes metodologias em sistemas fechados e abertos, para uma grande variedade de matrizes orgânicas, no sentido de se caracterizar com mais eficiência esses materiais que são largamente empregados na adubação das lavouras.…”
Section: Introductionunclassified
“…Contents of carbon, hydrogen, oxygen, nitrogen, and sulfur were obtained in a PerkinElmer 2400 Series II Elemental Analyzer. Metallic content (Al, As, B, Ba, Ca, Cd, Co, Cu, Fe, K, Mg, Mn, Mo, Ni, P, Pb, and Zn) was determined with an ICPE-9000 Multitype ICP Emission Spectrometer (Shi-madzu®, Tokyo, Japan) following the methods of Hseu et al [34]. Proximate analysis for moisture, volatile solids, ashes, and fixed carbon was carried out in a TGA7 Thermogravimetric Analyzer (PerkinElmer, Massachusetts, USA).…”
Section: Chemical Propertiesmentioning
confidence: 99%