2014
DOI: 10.1063/1.4878915
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A 31 T split-pair pulsed magnet for single crystal x-ray diffraction at low temperature

Abstract: We have developed a pulsed magnet system with panoramic access for synchrotron x-ray diffraction in magnetic fields up to 31 T and at low temperature down to 1.5 K. The apparatus consists of a split-pair magnet, a liquid nitrogen bath to cool the pulsed coil, and a helium cryostat allowing sample temperatures from 1.5 up to 250 K. Using a 1.15 MJ mobile generator, magnetic field pulses of 60 ms length were generated in the magnet, with a rise time of 16.5 ms and a repetition rate of 2 pulses/h at 31 T. The set… Show more

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Cited by 17 publications
(5 citation statements)
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“…Irreversible field-induced phase transitions have been previously observed by high-field susceptibility measurements in Fe 1.1 Te albeit at much higher temperatures and applied fields [34,35]. As a possible origin these authors suspected intrinsic magnetostructural changes [33] and detwinning.…”
Section: Discussionmentioning
confidence: 64%
“…Irreversible field-induced phase transitions have been previously observed by high-field susceptibility measurements in Fe 1.1 Te albeit at much higher temperatures and applied fields [34,35]. As a possible origin these authors suspected intrinsic magnetostructural changes [33] and detwinning.…”
Section: Discussionmentioning
confidence: 64%
“…By analogy, magn etic order induced by an external field may exist for x 0.06 ⩽ as well. Irreversible field-induced phase transitions have been previously observed by high-field susceptibility measurements in Fe 1.1 Te albeit at much higher temperatures and applied fields [33,34]. As a possible origin these authors suspected intrinsic magnetostructural changes [32] and detwinning.…”
Section: Discussionmentioning
confidence: 64%
“…For higher continuous fields, one has to resort to more permanent installations like Bitter magnets, very large superconductors, or hybrids of these two. Pulsed magnetic fields using capacitor banks are often transportable and split coils can reach up to 30 T [103][104][105] and solenoids up to 40 T [106], but the short pulses (msec) and the slow repetition rates (several shots/hour) make these magnets unrealistic options for soft matter research.…”
Section: Electromagnetic Fieldsmentioning
confidence: 99%