“…34,35 Meanwhile, the JCPDS 044-1481 conrmed that the dominant diffraction peak formed during the calcination at 1000 °C was Ca(OH) 2 with minor CaO peaks in the diffraction planes of (111) and (220) at 31.54°and 54.26°, respectively, based on JCPDS 037-1497. 35,36 The Ca(OH) 2 peak was dominant because the reaction in eqn (2) happened before the CaO was dissolved in distilled water. Aer calcination, the SL shells become more hygroscopic, which facilitates the samples' ability to absorb water from the air.…”