Monoisotopic mass spectra are given for the compounds: tetrameth yllead, t rim ethylethyllead, dimethyldiethyllead, methyltriethyllead, tetraethyllead, tetrapropylJ ead, trimethyl-n-butyllead, trimethyl-sec-butyllead, trimethyl-tert-butyllead, and tetra-isobutyllead. R elations between relative probabilities of ion formation and molecular structure are observed for several ion configurations and are discussed briefly.