A Comparison of NMR Spectra Obtained for Solid-Phase-Synthesis Resins Using Conventional High-Resolution, Magic-Angle-Spinning, and High-Resolution Magic-Angle-Spinning Probes

Structure elucidation of nanoparticle-bound organic molecules by 1H NMR

“…The high-resolution magic-angle spinning (HRMAS) NMR technique was successfully used in 1990s in combinatorial chemistry applications [59][60][61][62][63].…”

Anwendung der HR‐MAS‐1H‐NMR‐Spektroskopie zur Untersuchung der Wechselwirkungen zwischen Liganden und synthetischen Rezeptoren

“…Nach Filtration und Einengen der Reaktionslˆsung wird 1 a in kristalliner Form als Isomerengemisch rac/ meso-1 a (4:1) erhalten. MS (16 [21] Die Unterscheidung zwischen polaren und nichtpolaren Bindungsbeitr‰gen in Abh‰ngigkeit von der Lˆsungs-mittelzusammensetzung ist eines der Hauptziele weiterf¸h-render Untersuchungen.…”

Peer Reviewed: NMR Spectroscopy: Past and Present

“…Signal broadening due to magnetic susceptibility discontinuities across the region sampled by the receiver coil can be eliminated by rotating the sample at high speeds around an axis at the magic angle. MAS probes have also proven useful for measuring high-resolution NMR spectra of samples not amenable to standard liquid-phase methods, such as peptides and other compounds on solidphase synthesis resins (50).…”