2007
DOI: 10.1016/j.molcata.2006.11.002
|View full text |Cite
|
Sign up to set email alerts
|

A facile nuclear bromination of phenols and anilines using NBS in the presence of ammonium acetate as a catalyst

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
5

Citation Types

0
62
0
2

Year Published

2008
2008
2023
2023

Publication Types

Select...
5
2

Relationship

0
7

Authors

Journals

citations
Cited by 105 publications
(64 citation statements)
references
References 10 publications
0
62
0
2
Order By: Relevance
“…Isolation of this novel dimer by semipreparative HPLC yielded enough material for its investigation by NMR. From the 1 H, 19 F and 13 C NMR spectra the dimer was assigned structure 4 ( Fig. 1).…”
Section: Resultsmentioning
confidence: 99%
See 3 more Smart Citations
“…Isolation of this novel dimer by semipreparative HPLC yielded enough material for its investigation by NMR. From the 1 H, 19 F and 13 C NMR spectra the dimer was assigned structure 4 ( Fig. 1).…”
Section: Resultsmentioning
confidence: 99%
“…This suggests a symmetrical dimer. The signals for an ethyl carbamate group are found in the 13 C NMR spectrum at δ = 14.6 and 60.1 ppm. The 13 C NMR spectrum also shows the presence of four quaternary carbons in the pyridine ring.…”
Section: Resultsmentioning
confidence: 99%
See 2 more Smart Citations
“…The reaction time could be diminished from 1 hour to 5 minutes by adding 0.1 mol% NH 4 OAc to the reaction and using CH 3 CN as the solvent (Scheme 2). 6,11 This optimized bromination procedure also worked smoothly for the synthesis of 4-bromoquinolin-3-amine (10) starting from commercially available quinolin-3-amine (11) (Scheme 2). Scheme 2.…”
Section: Resultsmentioning
confidence: 99%