2005
DOI: 10.1016/j.powtec.2004.11.007
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A glass transition temperature approach for the prediction of the surface stickiness of a drying droplet during spray drying

Abstract: The development of surface stickiness of droplets of sugar and acid-rich foods during spray drying can be explained using the notion of glass transition temperature (T g). In this work, criteria for a safe drying regime have been developed and their physical basis provided. A dimensionless time (w) is introduced as an indicator of spray dryability and it is correlated with the recovery of powders in practical spray drying. Droplets with initial diameters of 120 Am were subjected to simulated spray drying condi… Show more

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Cited by 110 publications
(53 citation statements)
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“…The major physical and structural deteriorative reactions that occur during processing and storage of foods are collapse of structure during freeze-and vacuum-drying [18,93], stickiness of food powders during spray, hot air and fluidized bed drying and storage [4,18], caking of food powders during storage [62], crystallization of sugar [38,191] or loss of crispness [170]. Caking and crystallization are time-dependent and irreversible, while collapse and stickiness development are time-independent [18,124].…”
Section: Physical Stabilitymentioning
confidence: 99%
“…The major physical and structural deteriorative reactions that occur during processing and storage of foods are collapse of structure during freeze-and vacuum-drying [18,93], stickiness of food powders during spray, hot air and fluidized bed drying and storage [4,18], caking of food powders during storage [62], crystallization of sugar [38,191] or loss of crispness [170]. Caking and crystallization are time-dependent and irreversible, while collapse and stickiness development are time-independent [18,124].…”
Section: Physical Stabilitymentioning
confidence: 99%
“…Suspended droplet drying: Suspended droplet drying is the most common technique used to obtain drying kinetics data [2,3,17,27,55,99]. This technique is also used to study volatile retention [62] and morphology changes [5] during spray drying.…”
Section: Drying Kinetics Measurementmentioning
confidence: 99%
“…In capillary type the liquid is homogeneously distributed on the surface of the solid, creating a continuous liquid phase. Andhikari et al (2003) studied the stickiness for solutions of fructose and maltodextrin during the drying process. They related the molecular weight with the force required to separate the solution of fructose/maltodextrin from the contact surface.…”
Section: 4mentioning
confidence: 99%
“…As functional agent, inulin has been employed as excipient, additive, thickener, emulsifier, gelling agent, sugar and fat substitute, etc. From the point of view of phase stability, the most common problems presented during the handling of amorphous powders are stickiness, agglomeration, crystallization, loss of volatile compounds, and crush (Andhikari et al 2001;Kay and Nottingham 2008;Khalloufi et al 2000). Recently, the stability of inulin during the storage has been evaluated and related to the concepts of a w and Tg, where a w is expressed as the amount of water adsorbed per 100 g of dried sample.…”
Section: Phase Stabilitymentioning
confidence: 99%