2011
DOI: 10.1039/c1gc15808b
|View full text |Cite
|
Sign up to set email alerts
|

A more efficient synthesis of 4,4′,4′′-tricarboxy-2,2′:6′,2′′-terpyridine

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
1
1
1
1

Citation Types

0
25
0
1

Year Published

2012
2012
2017
2017

Publication Types

Select...
5
2
1

Relationship

1
7

Authors

Journals

citations
Cited by 34 publications
(26 citation statements)
references
References 30 publications
0
25
0
1
Order By: Relevance
“…The synthesis of 1-{4-[(hexyloxy)methyl]pyridin-2-yl}ethanone (3) is a two-step process, starting from alcohol derivative (1), which can be obtained either from methyl or ethyl 2-acetylisonicotinate [18][19][20] according to a procedure described in the literature [21] (Scheme 1). Deprotection of the ketone function was carried out in an acidic aqueous solution under reflux.…”
Section: Resultsmentioning
confidence: 99%
“…The synthesis of 1-{4-[(hexyloxy)methyl]pyridin-2-yl}ethanone (3) is a two-step process, starting from alcohol derivative (1), which can be obtained either from methyl or ethyl 2-acetylisonicotinate [18][19][20] according to a procedure described in the literature [21] (Scheme 1). Deprotection of the ketone function was carried out in an acidic aqueous solution under reflux.…”
Section: Resultsmentioning
confidence: 99%
“…In an industrial setting, multi-phase homogeneous catalysis is applied in the Rhône-Poulenc/Ruhrchemie process for aqueous biphasic hydroformylation [35]. Although general consensus suggests avoiding [40,41] or at least improving homogeneous catalysis via immobilization [42,43], a recent article showed how a novel organo-catalyzed synthesis is made more efficient than the original heterogeneous route (Scheme 3.9) [44].…”
Section: Opportunities In Homogeneous Catalysismentioning
confidence: 99%
“…This procedure was further improved by Dehaudt et al [55]. Among the other possible strategies to obtain a tpy core, it is worth noting an inverse Diels-Alder reaction on 1,2,4-triazine that uses 2,5-norbornadiene as dienophile [56].…”
Section: Synthesismentioning
confidence: 99%