“…They display exceptional performance in breaking down organic dyes and aiding in hydrogen generation, thanks to their distinct characteristics, such as narrow bandgaps and high catalytic efficiency. − Many techniques have been reported in the literature for producing nanosized spinel structures, which encompass Pechini sol–gel, sol–gel, microemulsion, coprecipitation, combustion, and sonochemical methods. ,− The Pechini sol–gel technique offers precise control over the composition, size, structure, and uniformity of the resulting product. − The spinel compound known as magnesium aluminate, with the chemical formula MgAl 2 O 4 , is frequently encountered. Its versatility has led to growing interest in multiple domains, including microwave dielectrics, refractory materials, humidity sensors, ceramic capacitors, structural materials for fusion reactors, and catalysis . Additionally, magnesium aluminate boasts advantageous properties, such as a high melting point (2135 °C), low density (3.58 g/cm 3 ), remarkable high-temperature strength, and outstanding resistance to chemical corrosion.…”