1996
DOI: 10.4028/www.scientific.net/msf.228-231.213
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A New White Beam Powder Diffraction Facility at the Daresbury Laboratory Synchrotron Radiation Source

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Cited by 18 publications
(11 citation statements)
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“…Intercalation reactions were performed in glass ampules contained within a temperaturecontrolled block, the details of which have been discussed previously. [21][22][23] A 0.5 g amount of the desired Al(OH) 3 polymorph was placed into an ampule with a magnetic stirrer bar. A 10 mL volume of the appropriate Li salt solution was added and the ampule sealed using a rubber septum.…”
Section: Methodsmentioning
confidence: 99%
“…Intercalation reactions were performed in glass ampules contained within a temperaturecontrolled block, the details of which have been discussed previously. [21][22][23] A 0.5 g amount of the desired Al(OH) 3 polymorph was placed into an ampule with a magnetic stirrer bar. A 10 mL volume of the appropriate Li salt solution was added and the ampule sealed using a rubber septum.…”
Section: Methodsmentioning
confidence: 99%
“…Powder X-ray diffraction patterns were recorded on a Siemens D5000 diffractometer equipped with a linear position-sensitive detector using Cu Kα 1 radiation in transmission geometry. In situ energy-dispersive X-ray diffraction data of the competition reactions were collected on Station 16.4 of the U.K. Synchrotron Radiation Source at Daresbury Laboratory using an experimental setup reported previously. , The guest solutions (approximately 0.1 M) were injected into an ampoule containing a suspension of [LiAl 2 (OH) 6 ]Cl·H 2 O at a rate of 0.2 mL/min from a SAGE Instruments syringe pump. Individual spectra were collected with acquisition times of 60 s and a fixed detector angle (2θ = 1.58°).…”
Section: Methodsmentioning
confidence: 99%
“…Details of both the SRS and the experimental setup are reported elsewhere. [26][27][28][29][30] EDXRD spectra were collected at a fixed detector angle of ca. 2u in 2h with an acquisition time of 30 s. The products were filtered, dried and characterized using X-ray powder diffraction, elemental analysis, IR spectroscopy, and thermogravimetric analysis.…”
Section: Characterisationmentioning
confidence: 99%