2009
DOI: 10.1016/j.apsusc.2009.08.080
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A novel one-step electron beam irradiation method for synthesis of Ag/Cu2O nanocomposites

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Cited by 49 publications
(27 citation statements)
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“…7c could be t into three main peaks locating at 529.6, 530.2 and 531.3 eV, which are ascribed to the Cu-O bond of CuO, lattice oxygen of Cu 2 O and surface-absorbed oxygen species (O 2 and H 2 O), respectively. 43,65,66 All the XPS analysis conrms the existence of both CuO and Cu 2 O in the sample V2.5 before and aer photodegradation under different conditions, in agreement with XRD results. In addition, the intensities of O 1s at 529.6 eV and 531.3 eV become gradually lower and higher in the absence and presence of H 2 O 2 for the degradation of MO, which demonstrates the decrease of CuO and increase of absorbed oxygen species on the surface of sample V2.5, respectively.…”
Section: Photocatalytic Activity Of As-grown Samplessupporting
confidence: 80%
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“…7c could be t into three main peaks locating at 529.6, 530.2 and 531.3 eV, which are ascribed to the Cu-O bond of CuO, lattice oxygen of Cu 2 O and surface-absorbed oxygen species (O 2 and H 2 O), respectively. 43,65,66 All the XPS analysis conrms the existence of both CuO and Cu 2 O in the sample V2.5 before and aer photodegradation under different conditions, in agreement with XRD results. In addition, the intensities of O 1s at 529.6 eV and 531.3 eV become gradually lower and higher in the absence and presence of H 2 O 2 for the degradation of MO, which demonstrates the decrease of CuO and increase of absorbed oxygen species on the surface of sample V2.5, respectively.…”
Section: Photocatalytic Activity Of As-grown Samplessupporting
confidence: 80%
“…7b, high resolution XPS spectrum in the Cu 2p 3/2 and Cu 2p 1/2 binding energy region shows the major peaks locating at 933.8 and 954.5 eV are in consistent with the reported value of CuO, while the peaks located at 932.5 and 952.6 eV are assigned to Cu 2 O. 18,64,65 The typical satellite peaks at 942 and 962.2 eV are also indexed to CuO 18,27,59,64,65 and the peaks showed slightly decrease aer photodegradation illustrating the decrease of CuO content on the surface of sample V2.5. The O 1s region in Fig.…”
Section: Photocatalytic Activity Of As-grown Samplessupporting
confidence: 79%
“…Electron‐beam produced voids and holes due to sputtering in thin films21 and in nanocomposite22,23 are also reported. Furthermore, electron beam lithography24 and radiolytic methods are common ways to achieve homogeneous and less aggregated nanoparticle composites from aqueous solutions of metal salts 25,26. The effect of high energy electron beam irradiation on 0‐3 nanocomposites is also mentioned in comparison with the influence of thermal annealing 27–30.…”
Section: Introductionmentioning
confidence: 99%
“…The tted peaks are originated from the lattice oxygen of adsorbed oxygen and Cu 2 O, respectively. 37,38 The XRD, EDS and XPS (as shown in Fig. 4(a), the ower-like hierarchical microspheres with a diameter about 3-4 mm are obtained when the molar ratio of Cu(NO 3 ) 2 $3H 2 O to AgNO 3 is 2.0 mmol/0.376 mmol.…”
Section: Resultsmentioning
confidence: 97%