“…The analytical technique mainly used for their determination in foods is liquid chromatography coupled with a photodiode array or mass spectrometer detector [ 12 ]. In fact, most of the scientific articles present in the literature used the liquid chromatography technique (HPLC) for the quantification of coumarin and oxygen heterocyclic compounds both in cinnamon-flavoured foods and in Citrus fruits [ 4 , 13 , 14 , 15 , 16 , 17 , 18 , 19 , 20 , 21 ]. Coumarin was generally quantified in cinnamon-flavoured bakery products, cereals, chocolate, milk and certainly in spices [ 13 , 16 ].…”