Gas-sofids circu fating fluidized beds have been successfully used in cata fytic cracking of heavy oil, coal combustion, and some metallurgical and physical processes (Grace, 1990). Gas-liquid-solids fluidized beds are operated mainly in conventional fluidization regimes without solids circulation or in the transport regime with low solids holdups (less than 5 % ) (Fan, 1989 (Berk et al., 1984). Circulating operation can promote solids mixing and increase product throughput per unit bed cross section, while high shear stress can promote biofilm renewal (Pirozzi et al., 1990
Experimental StudiesThe experimental apparatus is shown in Figure 1. The riser is 140-mm-dia., 3-m-high Plexiglas. Tap water and air were used as liquid and gas phases, respectively. Glass beads of 0.405 mm in mean diameter and density 2,460 kg/m3 were used as the solid phase. In the operation, fluidizing water was introduced from the base of the riser through a liquid distributor, while solids flow rate was regulated by a secondary water flow from a side port near the bottom of the riser. The superficial liquid velocity was calculated based on the total flow rate from both the liquid distributor and the secondary side port. Gas was introduced separately through a gas distributor located well above the bottom liquid distributor. Well-mixed threephase flow was achieved in the test section above the gas distributor. Solids entrained from the top of the riser was separated from the water and returned to a reservoir. The solids circulation rate was determined by measuring the amount of particles collected in a metering tank on the top of the standpipe after the butterfly valve beneath the metering tank was closed, similar to the method used in the gas-solids circulating fluidized bed (Burke11 et al., 1988).Local gas holdup was measured using an electrical conducCorrespondence concerning this article should be addressed to Y. Jin tivity probe. The tip of the probe was a 0.1-mm platinum wire, covered by a 0.2-mm glass tube. The probe was installed with the tip directed downward to minimize the disturbance of local flow patterns. Typical signals from the probe are shown in Figure 2. The output voltage is seen to drop sharply when bubbles pass the probe. The local bubble fraction can thus be determined by:where ti is the exposure time of the probe to bubbles and T is the total record time. The cross-sectional average gas holdup is calculated by:To evaluate the cross-sectional average solids holdup, pressure drops across the test section were also measured. The sectional average solids holdup is evaluated by combining Eqs. 2, 3 and 4: